2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propen-1-yl)-

Base Information

Chemical Name:2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propen-1-yl)-
CAS No.:104973-90-2
Molecular Formula:C₂₁H₂₂O₅
Molecular Weight:354.403
Hs Code.:

Synonyms:2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propenyl)-(9CI); 2,5-Cyclohexadien-1-one,4-[2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propenyl)-,(E)-(?à)-; Hancinone D

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Chemical Property of 2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propen-1-yl)-

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Technology Process of 2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propen-1-yl)-

There total 6 articles about 2,5-Cyclohexadien-1-one,4-[(1E)-2-(1,3-benzodioxol-5-yl)-1-methylethenyl]-4,5-dimethoxy-2-(2-propen-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 62499-71-2,62560-95-6,74163-93-2,74163-94-3,104973-89-9
isodihydrofutoquinol A

: 28178-92-9,104973-90-2
futoquinol

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 24h; Heating;
DOI:10.1016/S0040-4039(00)94967-0

Reference yield:

: 56879-12-0
1-(4-(benzyloxy)-2-methoxyphenyl)ethanone

: 28178-92-9,104973-90-2
futoquinol

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / n-BuLi / tetrahydrofuran / 1 h / -70 - -20 °C

2: 78 percent / Raney Ni / dioxane / 20 h / Heating

3: 1.) K₂CO₃ / 1.) acetone, reflux, 11 h, 2.) 125 grad C, 4 h

4: 51 percent / tetrahydrofuran / electrolyzis, glassy carbon anode, platinum cathode

5: 72 percent / DDQ / benzene / 24 h / Heating

With n-butyllithium; nickel; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1016/S0040-4039(00)94967-0

Reference yield:

: 56579-86-3
2-(3,4-methylenedioxyphenyl)-1,3-dithiane

: 28178-92-9,104973-90-2
futoquinol

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / n-BuLi / tetrahydrofuran / 1 h / -70 - -20 °C

2: 78 percent / Raney Ni / dioxane / 20 h / Heating

3: 1.) K₂CO₃ / 1.) acetone, reflux, 11 h, 2.) 125 grad C, 4 h

4: 51 percent / tetrahydrofuran / electrolyzis, glassy carbon anode, platinum cathode

5: 72 percent / DDQ / benzene / 24 h / Heating

With n-butyllithium; nickel; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1016/S0040-4039(00)94967-0