1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro-

Base Information

Chemical Name:1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro-
CAS No.:144062-76-0
Molecular Formula:C12H7BrCl2N2
Molecular Weight:330.00700
Hs Code.:2933990090
Mol file:144062-76-0.mol

Synonyms:1-(4-(Bromomethyl)phenyl)-3,5-dichloro-1H-pyrrole-2-carbonitrile;

Suppliers and Price of 1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(4-(Bromomethyl)phenyl)-3,5-dichloro-1H-pyrrole-2-carbonitrile 95+%
1g
$ 762.00

Chemenu
1-(4-(bromomethyl)phenyl)-3,5-dichloro-1H-pyrrole-2-carbonitrile 95%
1g
$ 720.00

Alichem
1-(4-(Bromomethyl)phenyl)-3,5-dichloro-1H-pyrrole-2-carbonitrile
1g
$ 607.60

Total 2 raw suppliers

Chemical Property of 1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro-

Chemical Property:

PSA：28.72000
LogP:4.55068

Purity/Quality:

95+% ^*data from raw suppliers

1-(4-(Bromomethyl)phenyl)-3,5-dichloro-1H-pyrrole-2-carbonitrile 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro-

There total 5 articles about 1H-Pyrrole-2-carbonitrile, 1-[4-(bromomethyl)phenyl]-3,5-dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142044-78-8
1-<4-(bromomethyl)phenyl>-1H-pyrrole-2-carbonitrile

: 144062-76-0
1-<4-(bromomethyl)phenyl>-3,5-dichloro-1H-pyrrole-2-carbonitrile

Guidance literature:: With N-chloro-succinimide; In methanol; chloroform;

Reference yield:

: 35524-48-2
1-(4-methylphenyl)pyrrole-2-carbonitrile

: 144062-76-0
1-<4-(bromomethyl)phenyl>-3,5-dichloro-1H-pyrrole-2-carbonitrile

Guidance literature:: With N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); Multistep reaction; 1.) CCl₄, reflux, 3 h, 2.) CHCl₃, MeOH, 16 h;
DOI:10.1021/jm00053a013

Reference yield:

: 827-60-1
1-(4-methylphenyl)-1H-pyrrole

: 144062-76-0
1-<4-(bromomethyl)phenyl>-3,5-dichloro-1H-pyrrole-2-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / 3 h / 110 - 120 °C

2: 1.) H₂NOH*HCl/Na₂CO₃, 2.) Ac₂O / 1.) MeOH, H₂O, reflux, 3 h, 2.) reflux, 3 h

3: 1.) N-bromosuccinimide, 2,2'-azobisisobutyronitrile, 2.) N-chlorosuccinimide / 1.) CCl₄, reflux, 3 h, 2.) CHCl₃, MeOH, 16 h

With N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydroxylamine hydrochloride; acetic anhydride; sodium carbonate; trichlorophosphate;
DOI:10.1021/jm00053a013