(17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside

Base Information

Chemical Name:(17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside
CAS No.:25517-69-5
Molecular Formula:C₂₄H₃₄O₇
Molecular Weight:434.53
Hs Code.:

Synonyms:Estra-1,3,5(10)-trien-3-ol,17a-(b-D-glucopyranosyloxy)- (8CI); Estrane, b-D-glucopyranoside deriv.;Glucopyranoside, 3-hydroxyestra-1,3,5(10)-trien-17a-yl, b-D- (8CI); 17a-Estradiol-17-glucoside; 17a-Estradiol-17-b-D-glucopyranoside

Suppliers and Price of (17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside

Chemical Property:

Vapor Pressure:4.07E-18mmHg at 25°C
Boiling Point:656.3°Cat760mmHg
Flash Point:350.7°C
Density:1.38g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside

There total 4 articles about (17beta)-3-hydroxyestra-1,3,5(10)-trien-17-yl beta-D-glycero-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 26041-33-8,26132-49-0,103596-10-7
17α-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)estra-1,3,5(10)-trien-3-yl acetate

: 25517-69-5
17α-(β-D-glucopyranosyloxy)estra-1,3,5(10)-trien-3-ol

Guidance literature:: With sodium methylate; In methanol; for 12h; Ambient temperature;
DOI:10.1135/cccc19920362

Reference yield:

: 15068-98-1
Acetic acid (8R,9S,13S,14S,17R)-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

: 25517-69-5
17α-(β-D-glucopyranosyloxy)estra-1,3,5(10)-trien-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieve 4A, silver silicate on silica gel / 1.) 100 Pa, 1 h, 2.) 1,2-dichloroethane, RT, 24 h

2: 93 percent / NaOMe / methanol / 12 h / Ambient temperature

With 4 A molecular sieve; silver silicate on silica gel; sodium methylate; In methanol;
DOI:10.1135/cccc19920362

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 25517-69-5
17α-(β-D-glucopyranosyloxy)estra-1,3,5(10)-trien-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieve 4A, silver silicate on silica gel / 1.) 100 Pa, 1 h, 2.) 1,2-dichloroethane, RT, 24 h

2: 93 percent / NaOMe / methanol / 12 h / Ambient temperature

With 4 A molecular sieve; silver silicate on silica gel; sodium methylate; In methanol;
DOI:10.1135/cccc19920362