Benzenepropanoic acid, a-[[hydroxy(phenylmethyl)phosphinyl]oxy]-, monomethyl ester, (R)-

Base Information

Chemical Name:Benzenepropanoic acid, a-[[hydroxy(phenylmethyl)phosphinyl]oxy]-, monomethyl ester, (R)-
CAS No.:144108-13-4
Molecular Formula:C₁₇H₁₉O₅P
Molecular Weight:334.309
Hs Code.:

Synonyms:

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Chemical Property of Benzenepropanoic acid, a-[[hydroxy(phenylmethyl)phosphinyl]oxy]-, monomethyl ester, (R)-

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Technology Process of Benzenepropanoic acid, a-[[hydroxy(phenylmethyl)phosphinyl]oxy]-, monomethyl ester, (R)-

There total 2 articles about Benzenepropanoic acid, a-[[hydroxy(phenylmethyl)phosphinyl]oxy]-, monomethyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6881-57-8
benzylphosphonic acid

: 144108-13-4
Methyl D-2-<(benzylhydroxyphosphoryl)oxy>-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 2) saponification

2: 1) triphenylphosphine, diisopropyl azodicarboxylate, 2) TMSBr / 1) THF, 1 h, 2) 1 h

With trimethylsilyl bromide; di-isopropyl azodicarboxylate; triphenylphosphine;
DOI:10.1021/jo00049a051

Reference yield:

: 63581-66-8
benzylphosphonic acid monomethyl ester

: 13673-95-5,13674-16-3,21632-25-7,27000-00-6
Methyl 3-L-phenyllactic acid

: 144108-13-4
Methyl D-2-<(benzylhydroxyphosphoryl)oxy>-3-phenylpropionate

Guidance literature:: With trimethylsilyl bromide; di-isopropyl azodicarboxylate; triphenylphosphine; Yield given. Multistep reaction; 1) THF, 1 h, 2) 1 h;
DOI:10.1021/jo00049a051