(7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol

Base Information

Chemical Name:(7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol
CAS No.:90370-97-1
Molecular Formula:C₈H₁₄O₃
Molecular Weight:158.197
Hs Code.:
NSC Number:191807
DSSTox Substance ID:DTXSID80307488
Nikkaji Number:J688.840B

Synonyms:90370-97-1;NSC191807;SCHEMBL9012552;7-oxabicyclo[2.2.1]heptane-2;DTXSID80307488;NSC-191807;7-oxabicyclo[2.2.1]heptane-2,3-diyldimethanol;(7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol

Suppliers and Price of (7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol

Chemical Property:

Vapor Pressure:0.00011mmHg at 25°C
Boiling Point:300.5°Cat760mmHg
Flash Point:135.6°C
Density:1.185g/cm³
XLogP3:-0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:158.094294304
Heavy Atom Count:11
Complexity:132

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C(C(C1O2)CO)CO

Technology Process of (7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol

There total 9 articles about (7-Oxabicyclo[2.2.1]heptane-2,3-diyl)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 81486-04-6,105761-77-1,106137-27-3,115888-24-9,133268-00-5
2-endo,3-exo-Bis(hydroxymethyl)-7-oxabicyclo<2.2.1>hept-5-ene

: 55423-53-5,68940-53-4,90370-97-1,97949-71-8,108691-75-4
(2-endo,3-exo)-7-oxabicyclo<2.2.1>heptane-2,3-dimethanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 2585.7 Torr;
DOI:10.1016/S0040-4020(01)87596-7

Reference yield: 62.0%

: 145-73-3,13136-04-4,28871-63-8,28874-46-6,97949-69-4,97949-70-7
(+)-7-Oxanorbornan-trans-2,3-dicarbonsaeure

: 55423-53-5,68940-53-4,90370-97-1,97949-71-8,108691-75-4
(2-endo,3-exo)-7-oxabicyclo<2.2.1>heptane-2,3-dimethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 55423-53-5,68940-53-4,90370-97-1,97949-71-8,108691-75-4
(2-endo,3-exo)-7-oxabicyclo<2.2.1>heptane-2,3-dimethanol

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous KOH-solution / anschliessend Behandeln mit Dimethylsulfat

2: lithium alanate; tetrahydrofuran

3: Raney nickel; ethyl acetate / Hydrogenation

With tetrahydrofuran; potassium hydroxide; lithium aluminium tetrahydride; nickel; ethyl acetate;