3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro-

Base Information

• Chemical Name: 3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro-
• CAS No.: 82670-73-3
• Molecular Formula: C₁₉H₁₄N₂O₆
• Molecular Weight: 366.33
• Mol file: 82670-73-3.mol

Synonyms:3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro-;82670-73-3

Chemical Property of 3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro-

Chemical Property:

• Vapor Pressure: 5.75E-11mmHg at 25°C
• Boiling Point: 521.3°Cat760mmHg
• Flash Point: 269.1°C
• Density: 1.426g/cm³
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 366.08518617
• Heavy Atom Count: 27
• Complexity: 687

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)N1C2=CC=CC=C2C(=O)C1=C(C3=CC=C(C=C3)[N+](=O)[O-])OC(=O)C
• Isomeric SMILES: CC(=O)N\1C2=CC=CC=C2C(=O)/C1=C(\C3=CC=C(C=C3)[N+](=O)[O-])/OC(=O)C

Technology Process of 3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro-

There total 4 articles about 3H-Indol-3-one, 1-acetyl-1-((acetyloxy)(4-nitrophenyl)methylene)-1,2-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

acetic anhydride (108-24-7) + 1-acetil-2-(4-nitrobenzoil)indolin-3-one (82670-67-5) → 1-acetil-2-(ossiacetil-4-nitrobenziliden)indolin-3-one (82670-73-3)

Guidance literature:

at 140 ℃; for 14h;

Reference yield: 35.0%

acetic anhydride (108-24-7) + 2-(4-nitrobenzoil)indolin-3-one (82670-63-1) → 1-acetil-2-(ossiacetil-4-nitrobenziliden)indolin-3-one (82670-73-3)

Guidance literature:

With potassium acetate; at 100 ℃; for 16h;

Reference yield:

N-(4-nitrofenacil)antranilato di metile (82670-58-4) → 1-acetil-2-(ossiacetil-4-nitrobenziliden)indolin-3-one (82670-73-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 65 percent

2: 78 percent / triethylamine / benzene

3: 41 percent / 14 h / 140 °C

With triethylamine; In benzene;

upstream raw materials:

acetic anhydride

2-(4-nitrobenzoil)indolin-3-one

1-acetil-2-(4-nitrobenzoil)indolin-3-one

N-(4-nitrofenacil)antranilato di metile