2(3H)-Thiophenone, dihydro-4,4-dimethyl-

Base Information

• Chemical Name: 2(3H)-Thiophenone, dihydro-4,4-dimethyl-
• CAS No.: 144303-84-4
• Molecular Formula: C6H10OS
• Molecular Weight: 130.211
• DSSTox Substance ID: DTXSID40481733
• Wikidata: Q82317326

Synonyms:2(3H)-Thiophenone, dihydro-4,4-dimethyl-;144303-84-4;SCHEMBL8734510;DTXSID40481733

Chemical Property of 2(3H)-Thiophenone, dihydro-4,4-dimethyl-

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 130.04523611
• Heavy Atom Count: 8
• Complexity: 118

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CC(=O)SC1)C

Technology Process of 2(3H)-Thiophenone, dihydro-4,4-dimethyl-

There total 1 articles about 2(3H)-Thiophenone, dihydro-4,4-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

Os3(CO)11(SCH2C(CH3)2CH2CO) → dodecacarbonyl triosmium (15696-40-9) + 4,4-dimethylthiobutyrolactone (144303-84-4) + Os2(CO)6(μ-SCH2C(Me)(CH2)CH2)(μ-H)

Guidance literature:

With CO; In ⁽²⁾H₈-toluene; High Pressure; soln. placed in an autoclave, sealed and pressurized with 1200 psi CO, heated to 120°C, after 16h the vessel was cooled and opened; addn. of CH2Cl2, lactone identified by NMR, evapn., chromd. (hexane/CH2Cl2 9/1);

DOI:10.1021/om00046a048

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