1H-Imidazole-5-carboxylic acid, 2-butyl-1-[[2'-[(1,1-dimethylethoxy)carbonyl][1,1'-biphenyl]-4-yl]methyl]-4- (1-hydroxy-1-methylethyl)-

Base Information

• Chemical Name: 1H-Imidazole-5-carboxylic acid, 2-butyl-1-[[2'-[(1,1-dimethylethoxy)carbonyl][1,1'-biphenyl]-4-yl]methyl]-4- (1-hydroxy-1-methylethyl)-
• CAS No.: 144690-48-2
• Molecular Formula: C29H36N2O5
• Molecular Weight: 492.615
• Mol file: 144690-48-2.mol

Synonyms:

Chemical Property of 1H-Imidazole-5-carboxylic acid, 2-butyl-1-[[2'-[(1,1-dimethylethoxy)carbonyl][1,1'-biphenyl]-4-yl]methyl]-4- (1-hydroxy-1-methylethyl)-

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Technology Process of 1H-Imidazole-5-carboxylic acid, 2-butyl-1-[[2'-[(1,1-dimethylethoxy)carbonyl][1,1'-biphenyl]-4-yl]methyl]-4- (1-hydroxy-1-methylethyl)-

There total 1 articles about 1H-Imidazole-5-carboxylic acid, 2-butyl-1-[[2'-[(1,1-dimethylethoxy)carbonyl][1,1'-biphenyl]-4-yl]methyl]-4- (1-hydroxy-1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate (144690-47-1) → 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylic acid (144690-48-2)

Guidance literature:

With lithium hydroxide monohydrate;

Reference yield:

1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylic acid (144690-48-2) + 4-bromomethyl-1,3-dioxa-5-methylcyclopentene-2-one (80715-22-6) → (5-Methyl-2-oxo-1,3-dioxolen-4yl)methyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate (144690-51-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide;

Reference yield:

1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylic acid (144690-48-2) + chloromethyl isopropyl carbonate (35180-01-9) → isopropoxycarbonyloxymethyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate (144690-50-6)

Guidance literature:

With potassium carbonate;

upstream raw materials:

methyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate

Downstream raw materials:

isopropoxycarbonyloxymethyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate

pivaloyloxymethyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate

(5-Methyl-2-oxo-1,3-dioxolen-4yl)methyl 1-[(2'-t-butoxycarbonylbiphenyl-4-yl)methyl]-2-butyl-4-(1-hydroxy-1-methylethyl)imidazole-5-carboxylate

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