6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine

Base Information

Chemical Name:6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine
CAS No.:73425-53-3
Molecular Formula:C₁₃H₁₆N₂S
Molecular Weight:232.349
Hs Code.:
DSSTox Substance ID:DTXSID40994156

Synonyms:BRN 5945627;6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine;4-(Aminomethyl)-6-methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole;Thiopyrano(2,3-b)indole-4-methylamine, 2,3,4,9-tetrahydro-6-methyl-;Thiopyrano(2,3-b)indole, 2,3,4,9-tetrahydro-4-(aminomethyl)-6-methyl-;73425-53-3;DTXSID40994156;LS-153276;1-(6-Methyl-2,3,4,9-tetrahydrothiopyrano[2,3-b]indol-4-yl)methanamine

Suppliers and Price of 6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine

Chemical Property:

Vapor Pressure:2.42E-07mmHg at 25°C
Boiling Point:422.4°Cat760mmHg
Flash Point:209.2°C
Density:1.228g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:232.10341969
Heavy Atom Count:16
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)NC3=C2C(CCS3)CN

Technology Process of 6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine

There total 5 articles about 6-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 73425-03-3
6-Methyl-2,3,4,9-tetrahydro-thiopyrano[2,3-b]indole-4-carbonitrile

: 73425-53-3
C-(6-Methyl-2,3,4,9-tetrahydro-thiopyrano[2,3-b]indol-4-yl)-methylamine

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride;
DOI:10.1248/cpb.32.877

Reference yield:

: 3484-35-3
5-methylindolin-2-one

: 73425-53-3
C-(6-Methyl-2,3,4,9-tetrahydro-thiopyrano[2,3-b]indol-4-yl)-methylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / P₂S₅, NaHCO₃ / tetrahydrofuran / 3 h / Ambient temperature

2: K₂CO₃

3: Heating

5: 46 percent / LiAlH₄-AlCl₃

With lithium aluminium tetrahydride; aluminium trichloride; tetraphosphorus decasulfide; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran;
DOI:10.1248/cpb.32.877

Reference yield:

: 73424-97-2
1,3-dihydro-5-methyl-2H-indole-2-thione

: 73425-53-3
C-(6-Methyl-2,3,4,9-tetrahydro-thiopyrano[2,3-b]indol-4-yl)-methylamine

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃

2: Heating

4: 46 percent / LiAlH₄-AlCl₃

With lithium aluminium tetrahydride; aluminium trichloride; potassium carbonate;
DOI:10.1248/cpb.32.877