Tin, [2,6-bis(1,1-dimethylethyl)-4-methylphenolato][1,1,1-trimethyl-N-(trimeth ylsilyl)silanaminato]-

Base Information

• Chemical Name: Tin, [2,6-bis(1,1-dimethylethyl)-4-methylphenolato][1,1,1-trimethyl-N-(trimeth ylsilyl)silanaminato]-
• CAS No.: 144877-34-9
• Molecular Formula: C₆H₁₈NSi₂*C₁₅H₂₃O*Sn
• Molecular Weight: 498.444

Synonyms:

Chemical Property of Tin, [2,6-bis(1,1-dimethylethyl)-4-methylphenolato][1,1,1-trimethyl-N-(trimeth ylsilyl)silanaminato]-

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Tin, [2,6-bis(1,1-dimethylethyl)-4-methylphenolato][1,1,1-trimethyl-N-(trimeth ylsilyl)silanaminato]-

There total 5 articles about Tin, [2,6-bis(1,1-dimethylethyl)-4-methylphenolato][1,1,1-trimethyl-N-(trimeth ylsilyl)silanaminato]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(CH3C6H2(C(CH3)3)2O)2Sn + 2C6H18NSi2(1-)*C12H28N2Si2(2-)*2Sn(2+) → {((CH3)3C)2C6H2(CH3)OSnNSi(CH3)3}2C6H10 + {Sn(N(Si(CH3)3)2)(OC6H2(C(CH3)3)2CH3)} (144877-34-9)

Guidance literature:

In toluene; stirred for 16 h at 25°C; not isolated as a solid, detn. by NMR;

Reference yield: 50.0%

(CH3C6H2(C(CH3)3)2O)2Sn + 2C6H18NSi2(1-)*C12H22N2Si2(2-)*2Sn(2+) → {((CH3)3C)2C6H2(CH3)OSnNSi(CH3)3}2C6H4 + {Sn(N(Si(CH3)3)2)(OC6H2(C(CH3)3)2CH3)} (144877-34-9)

Guidance literature:

In toluene; stirred for 16 h at 25°C; filtered, filtrate evapd., cooled to 5°C;

Reference yield:

[bis(trimethylsilyl)amino]tin chloride dimer + lithium 2,6-di-tert-butyl-4-methylphenoxide (42031-71-0) → {Sn(N(Si(CH3)3)2)(OC6H2(C(CH3)3)2CH3)} (144877-34-9)

Guidance literature:

In hexane; Sn compd. and LiOC6H2tBu2-2,6-Me-4 in n-C6H14 (25°C, 1 h);

DOI:10.1039/c39920001311

upstream raw materials:

lithium 2,6-di-tert-butyl-4-methylphenoxide

2,6-di-tert-butyl-4-methyl-phenol

bis(bis(trimethylsilyl)amido)tin(II)

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