Phosphonic acid, [(1E)-2-phenylethenyl]-, dibutyl ester

Base Information

Chemical Name:Phosphonic acid, [(1E)-2-phenylethenyl]-, dibutyl ester
CAS No.:146896-99-3
Molecular Formula:C16H25O3P
Molecular Weight:296.346
Hs Code.:
Mol file:146896-99-3.mol

Synonyms:

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Chemical Property of Phosphonic acid, [(1E)-2-phenylethenyl]-, dibutyl ester

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Technology Process of Phosphonic acid, [(1E)-2-phenylethenyl]-, dibutyl ester

There total 6 articles about Phosphonic acid, [(1E)-2-phenylethenyl]-, dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1809-19-4
dibutyl hydrogen phosphite

: (E)-phenylethenyl(phenyl)iodonium tetrafluoroborate

: 146896-99-3
dibutyl (E)-2-phenylethenylphosphonate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; copper(l) iodide; In tetrahydrofuran; N,N-dimethyl-formamide; at 35 ℃; for 15h;
DOI:10.1021/ol047516y

Reference yield: 67.0%

: 1809-19-4
dibutyl hydrogen phosphite

: 140-10-3
(E)-3-phenylacrylic acid

: 146896-99-3
dibutyl (E)-2-phenylethenylphosphonate

Guidance literature:: With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; silver(l) oxide; In dimethyl sulfoxide; at 120 ℃; for 12h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo501321m

Reference yield: 65.0%

: 1809-19-4
dibutyl hydrogen phosphite

: 5153-67-3
nitrostyrene

: 146896-99-3
dibutyl (E)-2-phenylethenylphosphonate

Guidance literature:: With silver nitrate; In acetonitrile; at 90 ℃; for 2h; stereoselective reaction; Schlenk technique;
DOI:10.1039/c6ra19002b