1,2,3,3a,4,5,5a,6,7,8-Decahydropyrene

Base Information

• Chemical Name: 1,2,3,3a,4,5,5a,6,7,8-Decahydropyrene
• CAS No.: 14698-02-3
• Molecular Formula: C₁₆H₂₀
• Molecular Weight: 212.335
• Mol file: 14698-02-3.mol

Synonyms:1,2,3,3a,4,5,5a,6,7,8-Decahydro-pyren;1,2,3,3a,4,5,5a,6,7,8-Decahydropyren;1,2,3,3a,4,5,5a,6,7,8-Dekahydropyren;1,2,3,3a,4,5,5a,6,7,8-decahydro-pyrene;1,2,3,4,5,6,7,8,12,13-decahydro-pyrene;

Chemical Property of 1,2,3,3a,4,5,5a,6,7,8-Decahydropyrene

Chemical Property:

• PSA: 0.00000
• LogP: 4.32020

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,3,3a,4,5,5a,6,7,8-Decahydropyrene

There total 6 articles about 1,2,3,3a,4,5,5a,6,7,8-Decahydropyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyrene (129-00-0) → perhydropyrene (2435-85-0,16291-77-3,41841-39-8,126188-36-1,126188-37-2,126188-38-3,126188-39-4,126188-40-7,126188-41-8,126188-42-9,126188-43-0,126188-44-1,126188-45-2,126188-46-3) + 1,2,3,3a,4,5,9,10,10a,10b-decahydropyrene (55821-21-1,55781-65-2,126188-30-5,53076-44-1) + 1,2,3,3a,4,5,5a,6,7,8-decahydropyrene (14698-02-3,69618-53-7,69618-54-8)

Guidance literature:

With hydrogen; In tetrahydrofuran; at 99.99 ℃; for 96.5h; under 11251.1 Torr; chemoselective reaction; Autoclave; Green chemistry;

DOI:10.1039/c3ra44871a

Reference yield:

pyrene (129-00-0) → perhydropyrene (2435-85-0,16291-77-3,41841-39-8,126188-36-1,126188-37-2,126188-38-3,126188-39-4,126188-40-7,126188-41-8,126188-42-9,126188-43-0,126188-44-1,126188-45-2,126188-46-3) + 1,2,3,3a,4,5,9,10,10a,10b-decahydropyrene (55821-21-1,55781-65-2,126188-30-5,53076-44-1) + 1,2,3,3a,4,5,5a,6,7,8-decahydropyrene (14698-02-3,69618-53-7,69618-54-8) + 1,2,3,3a,4,5,5a,6,7,8,8a,9,10,10a-tetradecahydropyrene (126117-26-8,126188-32-7,126188-33-8,126188-34-9,126188-35-0)

Guidance literature:

With hydrogen; at 20 ℃; for 0.5h; under 7600.51 Torr;

DOI:10.1039/c1nj20028c

Reference yield:

pyrene (129-00-0) → 4,5,9,10-tetrahydropyrene (781-17-9) + 1,2,3,6,7,8-hexahydropyrene (1732-13-4) + perhydropyrene (2435-85-0,16291-77-3,41841-39-8,126188-36-1,126188-37-2,126188-38-3,126188-39-4,126188-40-7,126188-41-8,126188-42-9,126188-43-0,126188-44-1,126188-45-2,126188-46-3) + 1,2,3,3a,4,5,9,10,10a,10b-decahydropyrene (55821-21-1,55781-65-2,126188-30-5,53076-44-1) + 1,2,3,3a,4,5,5a,6,7,8-decahydropyrene (14698-02-3,69618-53-7,69618-54-8) + 1,2,3,3a,4,5,5a,6,7,8,8a,9,10,10a-tetradecahydropyrene (126117-26-8,126188-32-7,126188-33-8,126188-34-9,126188-35-0)

Guidance literature:

With hydrogen; at 20 ℃; for 3h; under 7600.51 Torr;

DOI:10.1039/c1nj20028c

upstream raw materials:

4,5,9,10-tetrahydropyrene

pyrene

Downstream raw materials:

naphtho[2,3-e]pyrene

(6H-naphtho[2,1,8,7-defg]naphthacen-6-yl)-succinic acid

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