Technology Process of Allenolic acid
There total 6 articles about Allenolic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
for 3.5h;
under 2068.59 Torr;
DOI:10.1002/anie.200502675
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaHCO3 / (PPh3)2PdCl2 / 1-methyl-pyrrolidin-2-one / 13 h / 130 °C
2: H2 / Pd/C / tetrahydrofuran / 3.5 h / 2068.59 Torr
With
hydrogen; sodium hydrogencarbonate;
bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
DOI:10.1002/anie.200502675
- Guidance literature:
-
C14H14O3;
With
methanol; sodium hydroxide; water;
In
tetrahydrofuran;
for 6h;
With
hydrogenchloride;
In
tetrahydrofuran; water;
pH=7;
