Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-

Base Information

Chemical Name:Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-
CAS No.:147701-15-3
Molecular Formula:C35H33O2P
Molecular Weight:516.62
Hs Code.:
DSSTox Substance ID:DTXSID70453680
Nikkaji Number:J1.019.993J
Mol file:147701-15-3.mol

Synonyms:Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-;147701-15-3;DTXSID70453680;Diphenyl[2-methyl-3-(trityloxy)propyl]phosphine oxide

Suppliers and Price of Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-

Chemical Property:

XLogP3:7.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:10
Exact Mass:516.22181729
Heavy Atom Count:38
Complexity:651

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(COC(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3)CP(=O)(C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl-

There total 4 articles about Phosphine oxide, [2-methyl-3-(triphenylmethoxy)propyl]diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 76-83-5
trityl chloride

: 147701-14-2
2-(RS)-methyl-1-(diphenyl-phosphinoyl)-propan-3-ol

: 147701-15-3
3-diphenylphosphinoyl-2-methyl-1-triphenylmethoxypropane

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 20h; Ambient temperature;

Reference yield: 87.0%

: 26156-84-3
N-tritylpyridinium tetrafluoroborate

: 147701-14-2
2-(RS)-methyl-1-(diphenyl-phosphinoyl)-propan-3-ol

: 147701-15-3
3-diphenylphosphinoyl-2-methyl-1-triphenylmethoxypropane

Guidance literature:: In acetonitrile; for 20h; Ambient temperature;

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 147701-15-3
3-diphenylphosphinoyl-2-methyl-1-triphenylmethoxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) pyridine / 1) Et₂O, 0 deg C, 1.5 h, 2) toluene, reflux, 1 d

2: 1) NaBH₄, BF₃*OEt₂, 2) 3percent H₂O₂, 12percent aq. NaOH / 1) THF, r.t., 1 h, 2) 1 h

3: 87 percent / acetonitrile / 20 h / Ambient temperature

With pyridine; sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; In acetonitrile;