Benzene, 2-bromo-5-hexadecyl-1,3-dimethyl-

Base Information

Chemical Name:Benzene, 2-bromo-5-hexadecyl-1,3-dimethyl-
CAS No.:150619-65-1
Molecular Formula:C24H41Br
Molecular Weight:409.494
Hs Code.:
Mol file:150619-65-1.mol

Synonyms:

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Chemical Property of Benzene, 2-bromo-5-hexadecyl-1,3-dimethyl-

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Technology Process of Benzene, 2-bromo-5-hexadecyl-1,3-dimethyl-

There total 7 articles about Benzene, 2-bromo-5-hexadecyl-1,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.4%

: 4-n-hexadecyl-2,6-dimethylbenzenediazonium tetrafluoroborate

: 24273-80-1
4-n-hexadecyl-2,6-dimethylphenol

: 150619-65-1
4-n-hexadecyl-2,6-dimethylbromobenzene

Guidance literature:: With hydrogen bromide; cetyltrimethylammonim bromide; sodium bromide; Ambient temperature;
DOI:10.1021/ja00071a050

Reference yield:

: 36653-82-4,124-29-8
1-Hexadecanol

: 150619-65-1
4-n-hexadecyl-2,6-dimethylbromobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 18 percent / ZnCl₂ / 21 h / 260 °C

2: 1.) BF₃*Et₂O, 2.) tert-butyl nitrite / 1.) THF, -15 deg C, 2.) THF, 0 deg C, 6 h

3: 40.4 percent / NaBr, aq. HBr, cetyltrimethylammonium bromide <(CTA)Br> / Ambient temperature

With tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen bromide; cetyltrimethylammonim bromide; sodium bromide; zinc(II) chloride;
DOI:10.1021/ja00071a050

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 150619-65-1
4-n-hexadecyl-2,6-dimethylbromobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 18 percent / ZnCl₂ / 21 h / 260 °C

2: 1.) BF₃*Et₂O, 2.) tert-butyl nitrite / 1.) THF, -15 deg C, 2.) THF, 0 deg C, 6 h

3: 40.4 percent / NaBr, aq. HBr, cetyltrimethylammonium bromide <(CTA)Br> / Ambient temperature

With tert.-butylnitrite; boron trifluoride diethyl etherate; hydrogen bromide; cetyltrimethylammonim bromide; sodium bromide; zinc(II) chloride;
DOI:10.1021/ja00071a050