5-(2-Methoxyphenoxy)-2-(pyridin-4-yl)pyriMidine-4,6(1H,5H)-dione

Base Information

• Chemical Name: 5-(2-Methoxyphenoxy)-2-(pyridin-4-yl)pyriMidine-4,6(1H,5H)-dione
• CAS No.: 150728-08-8
• Molecular Formula: C16H13N3O4
• Molecular Weight: 311.29200
• Mol file: 150728-08-8.mol

Synonyms:5-(o-Methoxyphenoxy)-4,6-dihydroxy-2-(4-pyridyl)pyrimidine;5-(2-methoxy-phenoxy)-2-(pyridin-4-yl)-pyrimidine-4,6-diol;5-(o-methoxyphenoxy)4,6-dihydroxy-2-(4-pyridyl)pyrimidine;5-(o-methoxyphenoxy)-4,6-dihydroxy-2-(pyridin-4-yl)-pyrimidine;5-(2-methoxy-phenoxy)-2-(pyridin-4-yl)-pyrimidin-4,6-diol;

Chemical Property of 5-(2-Methoxyphenoxy)-2-(pyridin-4-yl)pyriMidine-4,6(1H,5H)-dione

Chemical Property:

• PSA: 97.59000
• LogP: 2.75070

Purity/Quality:

NLT 98% ^*data from raw suppliers

5-(o-Methoxyphenoxy)-4,6-dihydroxy-2-(4-pyridyl)pyrimidine 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 5-(2-Methoxyphenoxy)-2-(pyridin-4-yl)pyriMidine-4,6(1H,5H)-dione

There total 6 articles about 5-(2-Methoxyphenoxy)-2-(pyridin-4-yl)pyriMidine-4,6(1H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

CH3 COOH + 2-(2-Methoxyphenoxy)propanedioic acid diethyl ester (20730-58-9) → 5-(o-methoxyphenoxy)-4,6-dihydroxy-2-(pyridin-4-yl)-pyrimidine (150728-08-8)

Guidance literature:

With sodium; In methanol; 4-amidinopyridine hydrochloride; water;

Reference yield:

pyridine-4-carbonitrile (100-48-1) + 2-(2-Methoxyphenoxy)propanedioic acid diethyl ester (20730-58-9) + 4-amidinopyridine hydrochloride (6345-27-3,42518-06-9,61875-64-7) → 5-(o-methoxyphenoxy)-4,6-dihydroxy-2-(pyridin-4-yl)-pyrimidine (150728-08-8)

Guidance literature:

With ammonium chloride; sodium; In methanol;

Reference yield:

2-(2-Methoxyphenoxy)propanedioic acid diethyl ester (20730-58-9) + 4-amidinopyridine hydrochloride (6345-27-3,42518-06-9,61875-64-7) → 5-(o-methoxyphenoxy)-4,6-dihydroxy-2-(pyridin-4-yl)-pyrimidine (150728-08-8)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 18h;

DOI:10.1016/S0960-894X(02)01084-3

upstream raw materials:

2-(2-Methoxyphenoxy)propanedioic acid diethyl ester

4-amidinopyridine hydrochloride

pyridine-4-carbonitrile

methyl (2-methoxyphenoxy) ethanoate

Downstream raw materials:

C₂₃H₂₀ClN₅O₄S

C₂₅H₂₅N₅O₆S

4-tert-butyl-N-[6-(4-hydroxy-2-butynyloxy)-5-(o-methoxyphenoxy)-2-(pyridin-4-yl)-4-pyrimidinyl]-benzene sulfonamide

5-isopropyl-N-[6-(4-hydroxy-2-butynyloxy)-5-(o-methoxyphenoxy)-2-(4-pyridyl)-4-pyrimidinyl]-2-pyridine sulfonamide

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