Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester

Base Information

Chemical Name:Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester
CAS No.:153171-96-1
Molecular Formula:C13H23O4P
Molecular Weight:274.297
Hs Code.:
DSSTox Substance ID:DTXSID30452270
Nikkaji Number:J860.893H

Synonyms:153171-96-1;Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester;DTXSID30452270;1-Allyl-2-oxocyclohexylphosphonic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:274.13339621
Heavy Atom Count:18
Complexity:343

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(=O)(C1(CCCCC1=O)CC=C)OCC

Technology Process of Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester

There total 2 articles about Phosphonic acid, [2-oxo-1-(2-propenyl)cyclohexyl]-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1080-41-7
diethyl (2-oxocyclohexyl)phosphonate

: 106-95-6
allyl bromide

: 153171-96-1
diethyl 1-allyl-2-oxocyclohexylphosphonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; hexane; for 5h; Ambient temperature;
DOI:10.1016/S0040-4039(97)00975-1

Reference yield: 54.0%

: 1080-41-7
diethyl (2-oxocyclohexyl)phosphonate

: 106-95-6
allyl bromide

: (2-Allyloxy-cyclohex-1-enyl)-phosphonic acid diethyl ester

: 153171-96-1
diethyl 1-allyl-2-oxocyclohexylphosphonate

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 24h; Heating;
DOI:10.1055/s-1993-25972

Reference yield: 66.0%

: 153171-96-1
diethyl 1-allyl-2-oxocyclohexylphosphonate

: 94-66-6
2-allylcyclohexan-1-one

Guidance literature:: With lithium aluminium tetrahydride; lithium diisopropyl amide; THF, heptane, ethylbenzene, -78 deg C to room temp.; room temp., 30 min;
DOI:10.1016/S0040-4039(97)00975-1