1,3-Benzenedicarboxamide, N,N'-bis[2,3-bis(acetyloxy)propyl]-2,4,6-triiodo-5-[[(tetrahydro-2-furanyl) carbonyl]amino]-

Base Information

Chemical Name:1,3-Benzenedicarboxamide, N,N'-bis[2,3-bis(acetyloxy)propyl]-2,4,6-triiodo-5-[[(tetrahydro-2-furanyl) carbonyl]amino]-
CAS No.:153714-15-9
Molecular Formula:C27H32I3N3O12
Molecular Weight:971.277
Hs Code.:
Mol file:153714-15-9.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Benzenedicarboxamide, N,N'-bis[2,3-bis(acetyloxy)propyl]-2,4,6-triiodo-5-[[(tetrahydro-2-furanyl) carbonyl]amino]-

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Technology Process of 1,3-Benzenedicarboxamide, N,N'-bis[2,3-bis(acetyloxy)propyl]-2,4,6-triiodo-5-[[(tetrahydro-2-furanyl) carbonyl]amino]-

There total 4 articles about 1,3-Benzenedicarboxamide, N,N'-bis[2,3-bis(acetyloxy)propyl]-2,4,6-triiodo-5-[[(tetrahydro-2-furanyl) carbonyl]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 52449-98-6
tetrahydrofuran-2-carbonyl chloride

: 76801-94-0
5-amino-N,N'-bis[2,3-bis(acetyloxy)propyl]2,4,6-triiodo-1,3-benzenedicarboxamide

: 153714-15-9
N,N'-Bis[2,3-bis(acetyloxy)propyl]-2,4,6-tri-iodo-5-[[(tetrahydro-2-furanyl)carbonyl]-amino]-1,3-benzenedicarboxamide

Guidance literature:: In N,N-dimethyl acetamide; for 20h; Ambient temperature;
DOI:10.1016/0040-4020(96)00668-0

Reference yield:

: 76801-94-0
5-amino-N,N'-bis[2,3-bis(acetyloxy)propyl]2,4,6-triiodo-1,3-benzenedicarboxamide

: 153714-15-9
N,N'-Bis[2,3-bis(acetyloxy)propyl]-2,4,6-tri-iodo-5-[[(tetrahydro-2-furanyl)carbonyl]-amino]-1,3-benzenedicarboxamide

Guidance literature:: In tetrahydrofuran-2-carbonyl chloride; N,N-dimethyl acetamide; ethyl acetate;

Reference yield:

: 16874-33-2
tetrahydro-2-furancarboxylic acid

: 153714-15-9
N,N'-Bis[2,3-bis(acetyloxy)propyl]-2,4,6-tri-iodo-5-[[(tetrahydro-2-furanyl)carbonyl]-amino]-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / oxalyl chloride / 15 h / Ambient temperature

2: 86 percent / N,N-dimethyl-acetamide / 20 h / Ambient temperature

With oxalyl dichloride; In N,N-dimethyl acetamide;
DOI:10.1016/0040-4020(96)00668-0