Technology Process of 2-Butenoic acid, 4-phenyl-, 1,1-dimethylethyl ester, (2E)-
There total 7 articles about 2-Butenoic acid, 4-phenyl-, 1,1-dimethylethyl ester, (2E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride;
In
water;
at 20 ℃;
for 12h;
optical yield given as %de;
stereoselective reaction;
Micellar solution;
DOI:10.1021/ol800028x
- Guidance literature:
-
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; toluene-4-sulfonic acid;
In
water;
at 22 ℃;
for 12h;
Sealed vial;
Inert atmosphere;
DOI:10.1021/jo200746y
- Guidance literature:
-
tert-butyl diethylphosphonoacetate;
With
methylmagnesium bromide;
In
tetrahydrofuran; diethyl ether;
at 0 - 20 ℃;
for 0.5h;
phenylacetaldehyde;
In
tetrahydrofuran; diethyl ether;
for 3h;
Reflux;
DOI:10.1021/acs.joc.6b00362
