1,3-Benzenedicarboxamide, N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-[4-(hydroxymethyl)-2- oxo-3-oxazolidinyl]-2,4,6-triiodo-

Base Information

Chemical Name:1,3-Benzenedicarboxamide, N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-[4-(hydroxymethyl)-2- oxo-3-oxazolidinyl]-2,4,6-triiodo-
CAS No.:154921-15-0
Molecular Formula:C26H30I3N3O13
Molecular Weight:973.25
Hs Code.:
Mol file:154921-15-0.mol

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Chemical Property of 1,3-Benzenedicarboxamide, N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-[4-(hydroxymethyl)-2- oxo-3-oxazolidinyl]-2,4,6-triiodo-

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Technology Process of 1,3-Benzenedicarboxamide, N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-[4-(hydroxymethyl)-2- oxo-3-oxazolidinyl]-2,4,6-triiodo-

There total 7 articles about 1,3-Benzenedicarboxamide, N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-[4-(hydroxymethyl)-2- oxo-3-oxazolidinyl]-2,4,6-triiodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 154921-13-8
<3,5-bis<<<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>amino>carbonyl>-2,4,6-triiodophenyl>carbamic acid, oxyranylmethyl ester

: 154921-15-0
N,N'-bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<4-(hydroxymethyl)-2-oxo-3-oxazolidinyl>-1,3-benzenedicarboxamide

Guidance literature:: pyridine; at 75 ℃; for 2h;
DOI:10.1021/jo00085a023

Reference yield:

: 99-31-0
5-aminoisophthalic acid

: 154921-15-0
N,N'-bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<4-(hydroxymethyl)-2-oxo-3-oxazolidinyl>-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 7 steps

1: 74 percent / aq. potassium iododichloride / H₂O / 18 h / 55 - 60 °C

2: 92 percent / thionyl chloride

3: N,N-dimethyl-acetamide / 16 h / Ambient temperature

4: pyridine / 6 h / Ambient temperature

5: dioxane; toluene / 15 h / 60 °C

6: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

7: 70 percent / pyridine / 2 h / 75 °C

With pyridine; thionyl chloride; potassium dichloroiodate; pyridine; phenylmercuric acetate; In 1,4-dioxane; N,N-dimethyl acetamide; water; toluene;
DOI:10.1021/jo00085a023

Reference yield:

: 35453-19-1
2,4,6-triiodo-5-aminoisophthalic acid

: 154921-15-0
N,N'-bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<4-(hydroxymethyl)-2-oxo-3-oxazolidinyl>-1,3-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / thionyl chloride

2: N,N-dimethyl-acetamide / 16 h / Ambient temperature

3: pyridine / 6 h / Ambient temperature

4: dioxane; toluene / 15 h / 60 °C

5: phenylmercuric acetate / dioxane / 4 h / Ambient temperature

6: 70 percent / pyridine / 2 h / 75 °C

With pyridine; thionyl chloride; pyridine; phenylmercuric acetate; In 1,4-dioxane; N,N-dimethyl acetamide; toluene;
DOI:10.1021/jo00085a023