[2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER

Base Information

Chemical Name:[2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER
CAS No.:155301-82-9
Molecular Formula:C13H18N2O3
Molecular Weight:250.29400
Hs Code.:
Mol file:155301-82-9.mol

Synonyms:2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER;[2-(2-AMINO-PHENYL)-2-OXO-ETHYL-CARBAMIC ACID TERT-BUTYL ESTER;

Suppliers and Price of [2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
[2-(2-Amino-phenyl)-2-oxo-ethyl]-carbamicacidtert-butylester 96%
500mg
$ 525.00

J&W Pharmlab
[2-(2-Amino-phenyl)-2-oxo-ethyl]-carbamicacidtert-butylester 96%
1g
$ 998.00

Crysdot
tert-Butyl(2-(2-aminophenyl)-2-oxoethyl)carbamate 95+%
1g
$ 608.00

American Custom Chemicals Corporation
(2-(2-AMINO-PHENYL)-2-OXO-ETHYL)-CARBAMIC ACID TERT-BUTYL ESTER 96.00%
5MG
$ 503.99

Alichem
tert-Butyl(2-(2-aminophenyl)-2-oxoethyl)carbamate
1g
$ 504.90

Total 5 raw suppliers

Chemical Property of [2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER

Chemical Property:

Boiling Point:423.8±25.0 °C(Predicted)
PKA:10.80±0.46(Predicted)
PSA：81.42000
Density:1.147±0.06 g/cm3(Predicted)
LogP:2.94830

Purity/Quality:

97% ^*data from raw suppliers

[2-(2-Amino-phenyl)-2-oxo-ethyl]-carbamicacidtert-butylester 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER

There total 4 articles about [2-(2-AMINO-PHENYL)-2-OXO-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 155301-81-8
2-[N-(tert-butyloxycarbonyl)amino]-2'-nitroacetophenone

: 155301-82-9
2-[N-(tert-butyloxycarbonyl)amino]-2'-aminoacetophenone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; water; ethyl acetate; for 0.116667h; under 1344.6 Torr; Yield given;
DOI:10.1021/jm9608523

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 155301-82-9
2-[N-(tert-butyloxycarbonyl)amino]-2'-aminoacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 45 h / 25 °C

2: H₂ / 10percent Pd-C / ethanol; ethyl acetate; H₂O / 0.12 h / 1344.6 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/jm9608523

Reference yield:

: 524698-41-7
2-Nitro-α-amino-acetophenon

: 155301-82-9
2-[N-(tert-butyloxycarbonyl)amino]-2'-aminoacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 45 h / 25 °C

2: H₂ / 10percent Pd-C / ethanol; ethyl acetate; H₂O / 0.12 h / 1344.6 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/jm9608523