5-Nitro-2-phenylsulfonylmethylbenzaldehyde

Base Information

Chemical Name:5-Nitro-2-phenylsulfonylmethylbenzaldehyde
CAS No.:155534-53-5
Molecular Formula:C14H11NO5S
Molecular Weight:305.311
Hs Code.:
DSSTox Substance ID:DTXSID40447430
Nikkaji Number:J2.142.698I
Wikidata:Q82266300
Mol file:155534-53-5.mol

Synonyms:5-nitro-2-phenylsulfonylmethylbenzaldehyde;155534-53-5;SCHEMBL4176109;DTXSID40447430;OWQJSRUZDKLDPT-UHFFFAOYSA-N;5-nitro-2-phenylsufonylmethylbenzaldehyde;2-(Phenylsulfonylmethyl)-5-nitrobenzaldehyde

Suppliers and Price of 5-Nitro-2-phenylsulfonylmethylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5-Nitro-2-phenylsulfonylmethylbenzaldehyde

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:305.03579362
Heavy Atom Count:21
Complexity:473

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)CC2=C(C=C(C=C2)[N+](=O)[O-])C=O

Technology Process of 5-Nitro-2-phenylsulfonylmethylbenzaldehyde

There total 6 articles about 5-Nitro-2-phenylsulfonylmethylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 89303-40-2
2-(2-phenylsulfonylmethyl-5-nitrophenyl)-1,3-dioxolane

: 155534-53-5
5-nitro-2-((phenylsulfonyl)methyl)benzaldehyde

Guidance literature:: With sulfuric acid; at 100 ℃; for 1h;
DOI:10.1055/s-1994-35866

Reference yield: 87.0%

: (5-nitro-2-((phenylsulfonyl)methyl)phenyl)methanol

: 155534-53-5
5-nitro-2-((phenylsulfonyl)methyl)benzaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1039/c9ob01745c

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 155534-53-5
5-nitro-2-((phenylsulfonyl)methyl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / p-TsOH / toluene / Heating

2: 35 percent / KOH; DMSO / 23 °C

3: aq. AcOH / 5 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; In toluene;
DOI:10.1021/ja0449168