Carbamodithioic acid, dimethyl-, 1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)- 4-(3-phenoxyphenyl)butyl ester

Base Information

Chemical Name:Carbamodithioic acid, dimethyl-, 1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)- 4-(3-phenoxyphenyl)butyl ester
CAS No.:157126-17-5
Molecular Formula:C27H38N3O2PS2
Molecular Weight:531.723
Hs Code.:
Mol file:157126-17-5.mol

Carbamodithioic acid, dimethyl-,
1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)-
4-(3-phenoxyphenyl)butyl ester

Synonyms:

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Chemical Property of Carbamodithioic acid, dimethyl-, 1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)- 4-(3-phenoxyphenyl)butyl ester

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Technology Process of Carbamodithioic acid, dimethyl-, 1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)- 4-(3-phenoxyphenyl)butyl ester

There total 3 articles about Carbamodithioic acid, dimethyl-, 1-(octahydro-1,3-dimethyl-2-oxido-2H-1,3,2-benzodiazaphosphol-2-yl)- 4-(3-phenoxyphenyl)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68737-65-5
(R,R)-N,N'-dimethyl-1,2-diaminocyclohexane

: 157126-17-5
Dimethyl-dithiocarbamic acid (R)-1-((3aR,7aR)-1,3-dimethyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-4-(3-phenoxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Et₃N / toluene

2: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, from -78 deg C to RT

3: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, -90 deg C to -70 deg C

With n-butyllithium; triethylamine; In toluene;
DOI:10.1021/ja962505o

Reference yield:

: 146983-71-3
(3aR,7aR)-1,2,3-Trimethyl-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

: 157126-17-5
Dimethyl-dithiocarbamic acid (R)-1-((3aR,7aR)-1,3-dimethyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-4-(3-phenoxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, from -78 deg C to RT

2: 1.) n-BuLi / 1.) THF, -78 deg C, 2.) THF, -90 deg C to -70 deg C

With n-butyllithium;
DOI:10.1021/ja962505o

Reference yield:

: 137-26-8,93196-73-7
Thiram

: 157126-93-7
(3aR,7aR)-1,3-Dimethyl-2-[4-(3-phenoxy-phenyl)-butyl]-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

: 157238-96-5,178153-39-4
Dimethyl-dithiocarbamic acid (S)-1-((3aR,7aR)-1,3-dimethyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-4-(3-phenoxy-phenyl)-butyl ester

: 157126-17-5
Dimethyl-dithiocarbamic acid (R)-1-((3aR,7aR)-1,3-dimethyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-4-(3-phenoxy-phenyl)-butyl ester

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 2.) THF, -90 deg C to -70 deg C;
DOI:10.1021/ja962505o