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Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate

Base Information
  • Chemical Name:Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate
  • CAS No.:15738-08-6
  • Molecular Formula:C39H30IrO3P2.ClO4
  • Molecular Weight:900.284
  • Hs Code.:
Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate

Synonyms:Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate

Suppliers and Price of Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
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Total 5 raw suppliers
Chemical Property of Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate
Chemical Property:
Purity/Quality:

99.90% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate

There total 3 articles about Iridium(1+), tricarbonylbis(triphenylphosphine)-, perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With carbon monoxide; In tetrahydrofuran; a soln. of Ir-complex in THF was stirred under CO for 30 min, with CO flushing over the soln., finely ground AgClO4 was added, soln. was stirred for 20 min; solvent was removed under vac., residue extd. with CH2Cl2, pentane was added to the ext., ppt. collected, recrystd. from CH2Cl2-pentane;
DOI:10.1021/om00131a021
Guidance literature:
With CO; In dichloromethane; byproducts: 1,5-cyclooctadiene; at -30°C within 5 min;;
Guidance literature:
With CO; In neat (no solvent, solid phase); byproducts: 1,5-cyclooctadiene; 25°C, 24 h;;
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