Benzaldehyde, 3,4,5-tris(decyloxy)-

Base Information

Chemical Name:Benzaldehyde, 3,4,5-tris(decyloxy)-
CAS No.:160061-06-3
Molecular Formula:C37H66O4
Molecular Weight:574.929
Hs Code.:
Mol file:160061-06-3.mol

Synonyms:

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Chemical Property of Benzaldehyde, 3,4,5-tris(decyloxy)-

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Technology Process of Benzaldehyde, 3,4,5-tris(decyloxy)-

There total 10 articles about Benzaldehyde, 3,4,5-tris(decyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (3,4,5-tris(decyloxy)phenyl)methanol

: 160061-06-3
3,4,5-tris(decyloxy)benzaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1039/d0tc04839a

Reference yield:

: ethyl 3,4,5-tri(decyloxy) benzoate

: 160061-06-3
3,4,5-tris(decyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / tetrahydrofuran; methanol; water / Inert atmosphere; Reflux

1.2: pH 1 / Cooling with ice

2.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux

3.1: manganese(IV) oxide / chloroform / 20 °C / Inert atmosphere

With manganese(IV) oxide; lithium aluminium tetrahydride; potassium hydroxide; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1246/cl.2010.714

Reference yield:

: 112-29-8
1-bromo dodecane

: 160061-06-3
3,4,5-tris(decyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 90 - 100 °C / Inert atmosphere

2.1: potassium hydroxide / tetrahydrofuran; methanol; water / Inert atmosphere; Reflux

2.2: pH 1 / Cooling with ice

3.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux

4.1: manganese(IV) oxide / chloroform / 20 °C / Inert atmosphere

With manganese(IV) oxide; lithium aluminium tetrahydride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2010.714