[1,1'-Biphenyl]-2-sulfonamide, 4'-[[2-butyl-4,5-dihydro-4-oxo-5-(phenylmethyl)-3H-imidazo[4,5-c]pyridin -3-yl]methyl]-N-(1,1-dimethylethyl)-

Base Information

• Chemical Name: [1,1'-Biphenyl]-2-sulfonamide, 4'-[[2-butyl-4,5-dihydro-4-oxo-5-(phenylmethyl)-3H-imidazo[4,5-c]pyridin -3-yl]methyl]-N-(1,1-dimethylethyl)-
• CAS No.: 161862-36-8
• Molecular Formula: C₃₄H₃₈N₄O₃S
• Molecular Weight: 582.767
• Mol file: 161862-36-8.mol

Synonyms:

Chemical Property of [1,1'-Biphenyl]-2-sulfonamide, 4'-[[2-butyl-4,5-dihydro-4-oxo-5-(phenylmethyl)-3H-imidazo[4,5-c]pyridin -3-yl]methyl]-N-(1,1-dimethylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [1,1'-Biphenyl]-2-sulfonamide, 4'-[[2-butyl-4,5-dihydro-4-oxo-5-(phenylmethyl)-3H-imidazo[4,5-c]pyridin -3-yl]methyl]-N-(1,1-dimethylethyl)-

There total 3 articles about [1,1'-Biphenyl]-2-sulfonamide, 4'-[[2-butyl-4,5-dihydro-4-oxo-5-(phenylmethyl)-3H-imidazo[4,5-c]pyridin -3-yl]methyl]-N-(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-(2-Butyl-4-oxo-4,5-dihydro-imidazo[4,5-c]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide (161862-35-7) → 4'-(5-Benzyl-2-butyl-4-oxo-4,5-dihydro-imidazo[4,5-c]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide (161862-36-8)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1016/S0223-5234(97)84011-1

Reference yield:

2-butyl-4,5-dihydro-4-oxo-3H-imidazo<4,5-c>pyridine (133052-28-5) → 4'-(5-Benzyl-2-butyl-4-oxo-4,5-dihydro-imidazo[4,5-c]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide (161862-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature; overnight

2: KOt-Bu / dimethylformamide / 18 h / Ambient temperature

With potassium tert-butylate; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0223-5234(97)84011-1

Reference yield:

[[2'-[(t-Butylamino)sulfonyl]-1,1'-biphenyl-4-yl]methyl] bromide (138733-52-5) → 4'-(5-Benzyl-2-butyl-4-oxo-4,5-dihydro-imidazo[4,5-c]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide (161862-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature; overnight

2: KOt-Bu / dimethylformamide / 18 h / Ambient temperature

With potassium tert-butylate; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0223-5234(97)84011-1

upstream raw materials:

4'-(2-Butyl-4-oxo-4,5-dihydro-imidazo[4,5-c]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide

2-butyl-4,5-dihydro-4-oxo-3H-imidazo<4,5-c>pyridine

[[2'-[(t-Butylamino)sulfonyl]-1,1'-biphenyl-4-yl]methyl] bromide

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