5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one

Base Information

Chemical Name:5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one
CAS No.:16253-00-2
Molecular Formula:C₉H₈N₄OS
Molecular Weight:220.255
Hs Code.:
DSSTox Substance ID:DTXSID00494687
Nikkaji Number:J2.047.075E
Mol file:16253-00-2.mol

Synonyms:16253-00-2;5-phenylazo-2-thiohydantoin;DTXSID00494687;5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one

Suppliers and Price of 5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:220.04188206
Heavy Atom Count:15
Complexity:299

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N=NC2C(=O)NC(=S)N2

Technology Process of 5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one

There total 1 articles about 5-[(E)-Phenyldiazenyl]-2-sulfanylideneimidazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16253-00-2
5-(phenylazo)-2-thiohydantoin

Guidance literature:: entspr. 3-Phenylaminomethyl-Verb. (3a), Eg.;

Reference yield:

: 6018-89-9
nickel(II) acetate tetrahydrate

: 16253-00-2
5-(phenylazo)-2-thiohydantoin

: [Ni(OAc)2(5-(phenylazo)-2-thiohydantoin)(H₂O)2]*2H₂O

Guidance literature:: In ethanol; water; hot EtOH soln. of ligand and hot H2O-EtOH soln. of Ni(OAc)2*H2O with AcOH were mixed, refluxed for 3 h on water bath; concd. on rotary evaporator under reduced pressure, sepd., washed with H2O, warm EtOH, Et2O, dried in vacuo over CaCl2; elem. anal.;
DOI:10.1016/j.tca.2003.11.021

Reference yield:

: copper(II) choride dihydrate

: 16253-00-2
5-(phenylazo)-2-thiohydantoin

: [CuCl₂(5-(phenylazo)-2-thiohydantoin)H₂O]*H₂O

Guidance literature:: In ethanol; water; hot EtOH soln. of ligand and hot H2O-EtOH soln. of CuCl2*H2O were mixed,refluxed for 3 h on water bath; concd. on rotary evaporator under reduced pressure, sepd., washed with H2O, warm EtOH, Et2O, dried in vacuo over CaCl2; elem. anal.;
DOI:10.1016/j.tca.2003.11.021