2,6-Bis(tributylstannyl)pyridine

Base Information

Chemical Name:2,6-Bis(tributylstannyl)pyridine
CAS No.:163630-07-7
Molecular Formula:C29H57NSn2
Molecular Weight:661.20300
Hs Code.:2933399990
DSSTox Substance ID:DTXSID90463963
Wikidata:Q82289086
Mol file:163630-07-7.mol

Synonyms:2,6-bis(tributylstannyl)pyridine;163630-07-7;Tributyl-(6-tributylstannylpyridin-2-yl)stannane;DTXSID90463963;AKOS024463405;GS-6222;FT-0697787;A882559

Suppliers and Price of 2,6-Bis(tributylstannyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
2,6-Bis(tributylstannyl)pyridine 95%
5g
$ 785.00

American Custom Chemicals Corporation
2,6-BIS(TRIBUTYLSTANNYL)PYRIDINE 95.00%
5MG
$ 504.35

Alichem
2,6-Bis(tributylstannyl)pyridine
5g
$ 798.48

Total 15 raw suppliers

Chemical Property of 2,6-Bis(tributylstannyl)pyridine

Chemical Property:

PSA：13.60000
LogP:8.06810
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:20
Exact Mass:657.25291
Heavy Atom Count:32
Complexity:357

Purity/Quality:

97% ^*data from raw suppliers

2,6-Bis(tributylstannyl)pyridine 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=NC(=CC=C1)[Sn](CCCC)(CCCC)CCCC

Technology Process of 2,6-Bis(tributylstannyl)pyridine

There total 1 articles about 2,6-Bis(tributylstannyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 626-05-1
2,6-Dibromopyridine

: 1461-22-9
tributyltin chloride

: 163630-07-7
2,6-bis(tributylstannyl)pyridine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; dropwise addn. of BuLi to dibromopyridine (over 2 h, -90°C), stirring (-90°C, 2 h), addn. of Bu3SnCl (over 1 h, below -75°C), warming to room temp.; water addn., extn. of aq. layer (CH2Cl2), drying combined org. layers (MgSO4), evapn., repeated distn. (140-150°C/5E-6 Torr); elem. anal.;
DOI:10.1139/v97-020