3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid

Base Information

Chemical Name:3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid
CAS No.:165949-84-8
Molecular Formula:C14H19NO4
Molecular Weight:265.309
Hs Code.:2924299090
Mol file:165949-84-8.mol

Synonyms:3-(1-(N-tertbutoxycarbonyl)aminoethyl)benzoic acid;3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid;(S)-3-(1-TERT-BUTOXYCARBONYLAMINO-ETHYL)-BENZOIC ACID;Benzoic acid,3-[1-[[(1,1-dimethylethoxy)carbonyl]amino]ethyl];3-<1'-<(tert-butyloxycarbonyl)amino>ethyl>benzoic acid;

Suppliers and Price of 3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
3-(1-tert-Butoxycarbonylamino-ethyl)-benzoicacid 96%
250mg
$ 175.00

Crysdot
3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoicacid 95+%
1g
$ 406.00

Chemenu
3-(1-tert-Butoxycarbonylamino-ethyl)-benzoicacid 95%
1g
$ 380.00

American Custom Chemicals Corporation
3-(1-TERT-BUTOXYCARBONYLAMINO-ETHYL)-BENZOIC ACID 96.00%
5MG
$ 499.98

Alichem
3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoicacid
1g
$ 347.68

Acrotein
3-(1-Boc-aminoethyl)benzoicacid 97%
1g
$ 440.00

Acrotein
3-(1-Boc-aminoethyl)benzoicacid 97%
0.5g
$ 293.33

Acrotein
3-(1-Boc-aminoethyl)benzoicacid 97%
0.25g
$ 192.50

Total 8 raw suppliers

Chemical Property of 3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid

Chemical Property:

Boiling Point:429.6±38.0 °C(Predicted)
PKA:4.22±0.10(Predicted)
PSA：79.12000
Density:1.151±0.06 g/cm3(Predicted)
LogP:3.17490
Storage Temp.:2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3-(1-tert-Butoxycarbonylamino-ethyl)-benzoicacid 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid

There total 5 articles about 3-(1-((tert-Butoxycarbonyl)amino)ethyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 1187930-71-7
3-(1-amino-ethyl)-benzoic acid

: 165949-84-8,193150-14-0
3-<1'-<(tert-butyloxycarbonyl)amino>ethyl>benzoic acid

Guidance literature:: With triethylamine; In water; acetone; at 20 ℃; for 16h;

Reference yield: 62.0%

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 1391437-37-8,165949-85-9
3-(1-aminoethyl)benzoic acid hydrochloride

: 165949-84-8,193150-14-0
3-<1'-<(tert-butyloxycarbonyl)amino>ethyl>benzoic acid

Guidance literature:: With triethylamine; In water; acetone; at 20 ℃; for 16h;

Reference yield:

: 3-(1-(hydroxyimino)ethyl)benzoic acid

: 165949-84-8,193150-14-0
3-<1'-<(tert-butyloxycarbonyl)amino>ethyl>benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85.7 percent / H₂, conc. HCl / 10percent Pd/C / ethanol / 5 h / 1551.4 Torr

2: 57 percent / Et₃N / H₂O; acetone / 20 h

With hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; water; acetone;
DOI:10.1021/ja00087a007