1-Butanesulfinic acid, sodium salt

Base Information

• Chemical Name: 1-Butanesulfinic acid, sodium salt
• CAS No.: 16642-95-8
• Molecular Formula: C4H10O2S.Na
• Molecular Weight: 144.17
• Mol file: 16642-95-8.mol

Synonyms:

Chemical Property of 1-Butanesulfinic acid, sodium salt

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Butanesulfinic acid, sodium salt

There total 1 articles about 1-Butanesulfinic acid, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium 1-buthanethiolate (4779-86-6) → dibutyl disulfide (629-45-8) + butanesulfinic acid sodium salt (16642-95-8)

Guidance literature:

With oxygen; cobalt phthalocyanine catalyst (KS-1); In sodium hydroxide; at 40 ℃; for 0.666667h; Product distribution; other catalyst, other time, other temperature;

Reference yield: 90.0%

(3-(2,6-dimethylphenoxy)-1-cyclohexylideneprop-1-en-2-yl)-diphenylphosphine oxide + butanesulfinic acid sodium salt (16642-95-8) → (3-(butylsulfonyl)-3-cyclohexylideneprop-1-en-2-yl)diphenylphosphine oxide

Guidance literature:

With acetic acid; In dimethyl sulfoxide; at 20 ℃; for 11h;

DOI:10.1021/acs.joc.7b00813

Reference yield: 86.0%

3,4-dimethoxyphenylacetaldehyde (5703-21-9) + butanesulfinic acid sodium salt (16642-95-8) → (E)-4-(butylsulfonylvinyl)-1,2-dimethoxybenzene

Guidance literature:

3,4-dimethoxyphenylacetaldehyde; With acetic anhydride; In neat (no solvent); at 25 ℃; for 0.166667h;

butanesulfinic acid sodium salt; In neat (no solvent); at 25 ℃; for 4h; stereoselective reaction;

DOI:10.1055/s-0037-1610822

upstream raw materials:

sodium 1-buthanethiolate

Downstream raw materials:

p-nitrobenzyl 1-butanesulfinate

Butanethiosulfonic acid S-cyclohexyl ester

1-(butylsulfinyl)benzene

3-(butylthio)-2-phenylimidazo[1,2-α]pyridine

Refernces