Benzoic acid, 4-[[(8-ethyl-5,6,7,8-tetrahydro-8-hydroxy-5,5-dimethyl-2-naphthalenyl)[[2- (trimethylsilyl)ethoxy]methyl]amino]carbonyl]-, methyl ester

Base Information

• Chemical Name: Benzoic acid, 4-[[(8-ethyl-5,6,7,8-tetrahydro-8-hydroxy-5,5-dimethyl-2-naphthalenyl)[[2- (trimethylsilyl)ethoxy]methyl]amino]carbonyl]-, methyl ester
• CAS No.: 166978-05-8
• Molecular Formula: C29H41NO5Si
• Molecular Weight: 511.734

Synonyms:

Chemical Property of Benzoic acid, 4-[[(8-ethyl-5,6,7,8-tetrahydro-8-hydroxy-5,5-dimethyl-2-naphthalenyl)[[2- (trimethylsilyl)ethoxy]methyl]amino]carbonyl]-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-[[(8-ethyl-5,6,7,8-tetrahydro-8-hydroxy-5,5-dimethyl-2-naphthalenyl)[[2- (trimethylsilyl)ethoxy]methyl]amino]carbonyl]-, methyl ester

There total 2 articles about Benzoic acid, 4-[[(8-ethyl-5,6,7,8-tetrahydro-8-hydroxy-5,5-dimethyl-2-naphthalenyl)[[2- (trimethylsilyl)ethoxy]methyl]amino]carbonyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[2-(Trimethylsilyl)ethoxymethyl]-4-[[(5,6,7,8-tetrahydro-5,5-dimethyl-8-oxo-2-naphthalenyl)amino]carbonyl]benzoic acid, methyl ester (166978-04-7) + ethylmagnesium bromide (925-90-6) → N-[2-(Trimethylsilyl)ethoxymethyl]-4-[[(5,6,7,8-tetrahydro-5,5-dimethyl-8-ethyl-8-hydroxy-2-naphthalenyl)amino]carbonyl]benzoic acid, methyl ester (166978-05-8)

Guidance literature:

In tetrahydrofuran; diethyl ether; hexane;

Reference yield:

→ N-[2-(Trimethylsilyl)ethoxymethyl]-4-[[(5,6,7,8-tetrahydro-5,5-dimethyl-8-ethyl-8-hydroxy-2-naphthalenyl)amino]carbonyl]benzoic acid, methyl ester (166978-05-8)

Guidance literature:

Reference yield:

p-toluenesulfonic acid (pTsOH) monohydrate + N-[2-(Trimethylsilyl)ethoxymethyl]-4-[[(5,6,7,8-tetrahydro-5,5-dimethyl-8-ethyl-8-hydroxy-2-naphthalenyl)amino]carbonyl]benzoic acid, methyl ester (166978-05-8) → 4-[[(5,6-Dihydro-5,5-dimethyl-8-ethyl-2-napthalenyl)amino]carbonyl]benzoic acid, methyl ester (166977-17-9)

Guidance literature:

In hexane; toluene;

upstream raw materials:

N-[2-(Trimethylsilyl)ethoxymethyl]-4-[[(5,6,7,8-tetrahydro-5,5-dimethyl-8-oxo-2-naphthalenyl)amino]carbonyl]benzoic acid, methyl ester

ethylmagnesium bromide

Downstream raw materials:

4-[[(5,6-Dihydro-5,5-dimethyl-8-ethyl-2-napthalenyl)amino]carbonyl]benzoic acid, methyl ester

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