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Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester

Base Information Edit
  • Chemical Name:Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester
  • CAS No.:167483-90-1
  • Molecular Formula:C21H24N2O2
  • Molecular Weight:336.434
  • Hs Code.:
  • Mol file:167483-90-1.mol
Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-,
phenylmethyl ester

Synonyms:

Suppliers and Price of Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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  • Chemicals and raw materials
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Total 1 raw suppliers
Chemical Property of Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester Edit
Chemical Property:
Purity/Quality:

99.90% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester

There total 2 articles about Spiro[3H-indole-3,4'-piperidine]-1(2H)-carboxylic acid, 1'-methyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 5 steps
1: 1.) ClCO2CHClCH3 / 1.) 1,2-dichloroethane, reflux, 1 h, 2.) MeOH, reflux, 1 h
2: EDC, HOBT, N-methylmorpholine / 12 h / Ambient temperature
3: TFA
4: EDC, HOBT / CH2Cl2 / 12 h / Ambient temperature
5: H2, Et3N / 10percent Pd/C / ethanol
With 4-methyl-morpholine; carbonochloridic acid 1-chloro-ethyl ester; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm960054c
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