2,4,8,10-Tetraazatridecanedioic acid, 10-[(3,4-dihydro-5-methyl-2,4-dioxo-1(2H)-pyrimidinyl)acetyl]-7-oxo-4-[[ 6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-9-yl]acetyl]-, 1-(1,1-dimethylethyl) 13-ethyl ester

Base Information

• Chemical Name: 2,4,8,10-Tetraazatridecanedioic acid, 10-[(3,4-dihydro-5-methyl-2,4-dioxo-1(2H)-pyrimidinyl)acetyl]-7-oxo-4-[[ 6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-9-yl]acetyl]-, 1-(1,1-dimethylethyl) 13-ethyl ester
• CAS No.: 171855-90-6
• Molecular Formula: C37H47N11O11
• Molecular Weight: 821.847

Synonyms:

Chemical Property of 2,4,8,10-Tetraazatridecanedioic acid, 10-[(3,4-dihydro-5-methyl-2,4-dioxo-1(2H)-pyrimidinyl)acetyl]-7-oxo-4-[[ 6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-9-yl]acetyl]-, 1-(1,1-dimethylethyl) 13-ethyl ester

Chemical Property:

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Technology Process of 2,4,8,10-Tetraazatridecanedioic acid, 10-[(3,4-dihydro-5-methyl-2,4-dioxo-1(2H)-pyrimidinyl)acetyl]-7-oxo-4-[[ 6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-9-yl]acetyl]-, 1-(1,1-dimethylethyl) 13-ethyl ester

There total 1 articles about 2,4,8,10-Tetraazatridecanedioic acid, 10-[(3,4-dihydro-5-methyl-2,4-dioxo-1(2H)-pyrimidinyl)acetyl]-7-oxo-4-[[ 6-[[(phenylmethoxy)carbonyl]amino]-9H-purin-9-yl]acetyl]-, 1-(1,1-dimethylethyl) 13-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H20N4O5*H(1+) + N-(N-tert-butyloxycarbonylaminomethyl)-N-(N9-benzyloxycarbonyladenin-9-ylacetyl)-β-alanine (171855-80-4) → 3-{({3-[[2-(6-Benzyloxycarbonylamino-purin-9-yl)-acetyl]-(tert-butoxycarbonylamino-methyl)-amino]-propionylamino}-methyl)-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-propionic acid ethyl ester (171855-90-6)

Guidance literature:

With pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; Yield given;

DOI:10.1016/0040-4039(95)01375-R

Reference yield: 96.0%

3-{({3-[[2-(6-Benzyloxycarbonylamino-purin-9-yl)-acetyl]-(tert-butoxycarbonylamino-methyl)-amino]-propionylamino}-methyl)-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-propionic acid ethyl ester (171855-90-6) → 3-{({3-[[2-(6-Benzyloxycarbonylamino-purin-9-yl)-acetyl]-(tert-butoxycarbonylamino-methyl)-amino]-propionylamino}-methyl)-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-propionic acid

Guidance literature:

With lithium hydroxide; In tetrahydrofuran;

DOI:10.1016/0040-4039(95)01375-R

Reference yield:

3-{({3-[[2-(6-Benzyloxycarbonylamino-purin-9-yl)-acetyl]-(tert-butoxycarbonylamino-methyl)-amino]-propionylamino}-methyl)-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-propionic acid ethyl ester (171855-90-6) → 3-{[(3-{Aminomethyl-[2-(6-benzyloxycarbonylamino-purin-9-yl)-acetyl]-amino}-propionylamino)-methyl]-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-propionic acid ethyl ester

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.333333h;

DOI:10.1016/0040-4039(95)01375-R

upstream raw materials:

N-(N-tert-butyloxycarbonylaminomethyl)-N-(N⁹-benzyloxycarbonyladenin-9-ylacetyl)-β-alanine

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