2,4-Thiazolidinedione, 5-[[4-[(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methoxy]phenyl] methyl]-3-(triphenylmethyl)-

Base Information

Chemical Name:2,4-Thiazolidinedione, 5-[[4-[(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methoxy]phenyl] methyl]-3-(triphenylmethyl)-
CAS No.:172648-23-6
Molecular Formula:C37H29ClN4O3S
Molecular Weight:645.181
Hs Code.:
Mol file:172648-23-6.mol

Synonyms:

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Chemical Property of 2,4-Thiazolidinedione, 5-[[4-[(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methoxy]phenyl] methyl]-3-(triphenylmethyl)-

Chemical Property:

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Technology Process of 2,4-Thiazolidinedione, 5-[[4-[(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methoxy]phenyl] methyl]-3-(triphenylmethyl)-

There total 4 articles about 2,4-Thiazolidinedione, 5-[[4-[(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methoxy]phenyl] methyl]-3-(triphenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150556-72-2
5-(4-hydroxy-benzyl)-3-triphenylmethylthiazolidine-2,4-dione

: 172648-22-5
(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-yl)methanol

: 172648-23-6
5-[4-(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In toluene; at 20 ℃; for 5h;
DOI:10.1021/jm990522t

Reference yield:

: 25710-20-7
5-chloro-2,3-diaminopyridine

: 172648-23-6
5-[4-(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 h / 150 °C

2.1: NaH / dimethylformamide / 1 h / 20 °C

2.2: dimethylformamide / 2 h / 20 °C

3.1: azodicarbonyldipieridine; Bu₃P / toluene / 5 h / 20 °C

With tributylphosphine; sodium hydride; 1,1'-azodicarbonyl-dipiperidine; In N,N-dimethyl-formamide; toluene; 1.1: Cyclization / 2.1: Metallation / 2.2: Alkylation / 3.1: Mitsunobu reaction;
DOI:10.1021/jm990522t

Reference yield:

: 91371-83-4
(6-chloro-3H-imidazo[4,5-b]pyridin-2-yl)methanol

: 172648-23-6
5-[4-(6-chloro-3-methyl-3H-imidazo[4,5-b]pyridin-2-ylmethoxy)benzyl]-3-triphenylmethylthiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 1 h / 20 °C

1.2: dimethylformamide / 2 h / 20 °C

2.1: azodicarbonyldipieridine; Bu₃P / toluene / 5 h / 20 °C

With tributylphosphine; sodium hydride; 1,1'-azodicarbonyl-dipiperidine; In N,N-dimethyl-formamide; toluene; 1.1: Metallation / 1.2: Alkylation / 2.1: Mitsunobu reaction;
DOI:10.1021/jm990522t