1,2-Ethanediol, 1-(2,4-dimethylphenyl)-, (1R)-

Base Information

Chemical Name:1,2-Ethanediol, 1-(2,4-dimethylphenyl)-, (1R)-
CAS No.:173171-01-2
Molecular Formula:C10H14O2
Molecular Weight:166.22
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Ethanediol, 1-(2,4-dimethylphenyl)-, (1R)-

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Technology Process of 1,2-Ethanediol, 1-(2,4-dimethylphenyl)-, (1R)-

There total 1 articles about 1,2-Ethanediol, 1-(2,4-dimethylphenyl)-, (1R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2234-20-0
2,4-dimethylstyrene

: 173171-01-2
(R)-1-(2,4-dimethylphenyl)-1,2-ethanediol

Guidance literature:: With potassium osmate(VI); potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 12h;
DOI:10.1021/jo00131a022

Reference yield:

: 173171-01-2
(R)-1-(2,4-dimethylphenyl)-1,2-ethanediol

: 173171-07-8
(R)-1-(2,4-dimethylphenyl)-2-(1-piperidinyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) TMSCl, CH₃C(OMe)3, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) MeOH, room temperature, 2 h

2: 73 percent / ethanol / 3 h / Heating

With Trimethyl orthoacetate; chloro-trimethyl-silane; potassium carbonate; In ethanol;
DOI:10.1021/jo00131a022

Reference yield:

: 173171-01-2
(R)-1-(2,4-dimethylphenyl)-1,2-ethanediol

: (R)-N-methyl-1-(2,4-dimethylphenyl)-2-(1-piperidinyl)ethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) TMSCl, CH₃C(OMe)3, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) MeOH, room temperature, 2 h

2: 73 percent / ethanol / 3 h / Heating

3: Et₃N / diethyl ether / 0.5 h

4: Et₃N / CH₂Cl₂; H₂O

With Trimethyl orthoacetate; chloro-trimethyl-silane; potassium carbonate; triethylamine; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/jo00131a022