N-[2-(2-Amino-1H-imidazole-4-yl)ethyl]-α-(hydroxyimino)-3,5-dibromo-4-methoxybenzenepropanamide

Base Information

• Chemical Name: N-[2-(2-Amino-1H-imidazole-4-yl)ethyl]-α-(hydroxyimino)-3,5-dibromo-4-methoxybenzenepropanamide
• CAS No.: 105596-36-9
• Molecular Formula: C15H17 Br2 N5 O3
• Molecular Weight: 475.14
• Mol file: 105596-36-9.mol

Synonyms:Ianthellin;Ianthelline

Chemical Property of N-[2-(2-Amino-1H-imidazole-4-yl)ethyl]-α-(hydroxyimino)-3,5-dibromo-4-methoxybenzenepropanamide

Chemical Property:

• PSA: 126.35000
• LogP: 2.57810

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[2-(2-Amino-1H-imidazole-4-yl)ethyl]-α-(hydroxyimino)-3,5-dibromo-4-methoxybenzenepropanamide

There total 2 articles about N-[2-(2-Amino-1H-imidazole-4-yl)ethyl]-α-(hydroxyimino)-3,5-dibromo-4-methoxybenzenepropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

(E)-N-(2-(2-amino-1H-imidazol-5-yl)ethyl)-3-(3,5-dibromo-4-methoxyphenyl)-2-(4-methoxybenzyloxyimino)propanamide (1248588-80-8) → (E)-N-(2-(2-amino-1H-imidazol-5-yl)ethyl)-3-(3,5-dibromo-4-methoxyphenyl)-2-(hydroxyimino)propanamide (105596-36-9)

Guidance literature:

With aluminum (III) chloride; methoxybenzene; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tetlet.2010.07.016

Reference yield:

→ aeroplysinine-1 (66141-25-1) + ianthelline (105596-36-9)

Guidance literature:

In methanol; chloroform; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)84977-1

Reference yield:

acetic anhydride (108-24-7) + ianthelline (105596-36-9) → C23H25Br2N5O7

Guidance literature:

With pyridine; at 50 ℃;

DOI:10.1016/S0040-4039(00)84977-1

upstream raw materials:

(E)-N-(2-(2-amino-1H-imidazol-5-yl)ethyl)-3-(3,5-dibromo-4-methoxyphenyl)-2-(4-methoxybenzyloxyimino)propanamide

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