1-(3-BROMOBENZYL)-1H-INDOLE-3-CARBALDEHYDE

Base Information

• Chemical Name: 1-(3-BROMOBENZYL)-1H-INDOLE-3-CARBALDEHYDE
• CAS No.: 174367-69-2
• Molecular Formula: C16H12BrNO
• Molecular Weight: 314.181
• Mol file: 174367-69-2.mol

Synonyms:N-(3-bromobenzyl)indole-3-carboxaldehyde;N-(m-bromobenzyl)indole-3-carboxaldehyde;1-(3-Bromo-benzyl)-1H-indole-3-carbaldehyde;1-(3-bromobenzyl)-1H-indole-3-carbaldehyde;

Chemical Property of 1-(3-BROMOBENZYL)-1H-INDOLE-3-CARBALDEHYDE

Chemical Property:

• Melting Point: 100 - 101 °C (benzene)
• PSA: 22.00000
• LogP: 4.26460

Purity/Quality:

98%min ^*data from raw suppliers

1-(3-Bromobenzyl)-1H-indole-3-carbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-(3-BROMOBENZYL)-1H-INDOLE-3-CARBALDEHYDE

There total 2 articles about 1-(3-BROMOBENZYL)-1H-INDOLE-3-CARBALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Indole-3-carboxaldehyde (487-89-8,1228547-52-1) + meta-bromobenzyl bromide (823-78-9) → 1-[(3-bromophenyl)methyl]-1H-indole-3-carboxaldehyde (174367-69-2)

Guidance literature:

With caesium carbonate; In acetonitrile; for 3h; Heating;

Reference yield: 57.0%

Indole-3-carboxaldehyde (487-89-8,1228547-52-1) → 1-[(3-bromophenyl)methyl]-1H-indole-3-carboxaldehyde (174367-69-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

Reference yield: 93.0%

1-[(3-bromophenyl)methyl]-1H-indole-3-carboxaldehyde (174367-69-2) → 1-[(3-bromophenyl)methyl]-1H-indole-3-methanol (210426-42-9)

Guidance literature:

With sodium tetrahydroborate;

upstream raw materials:

Indole-3-carboxaldehyde

meta-bromobenzyl bromide

Downstream raw materials:

1-[(3-bromophenyl)methyl]-1H-indole-3-methanol

bis[1-[(3-bromophenyl)methyl]-1H-indole-3-]methane

(E)-3-(1-(3-bromobenzyl)-1H-indol-3-yl)-1-(5-methoxy-2,2-dimethyl-2H-chromen-8-yl)prop-2-en-1-one

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