3-ACETOXY-4-METHYLBENZOIC ACID

Base Information

• Chemical Name: 3-ACETOXY-4-METHYLBENZOIC ACID
• CAS No.: 17477-46-2
• Molecular Formula: C10H10O4
• Molecular Weight: 194.187
• Hs Code.: 2918990090
• Mol file: 17477-46-2.mol

Synonyms:3-acetyloxy-4-methyl-benzoic acid;3-acetoxy-4-methylbenzoic acid;3-Acetoxy-4-methyl-benzoesaeure;

Chemical Property of 3-ACETOXY-4-METHYLBENZOIC ACID

Chemical Property:

• PSA: 63.60000
• LogP: 1.61850
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Acetoxy-4-methylbenzoicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ACETOXY-4-METHYLBENZOIC ACID

There total 2 articles about 3-ACETOXY-4-METHYLBENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.3%

3-hydroxy-4-methylbenzoic acid (586-30-1) + acetic anhydride (108-24-7) → 3-acetyloxy-4-methylbenzoic acid (17477-46-2)

Guidance literature:

for 5h; Heating / reflux;

Reference yield:

→ 3-acetyloxy-4-methylbenzoic acid (17477-46-2)

Guidance literature:

Hydroxy-Verb. IXg, Acetanhydrid;

DOI:10.1007/BF00928603

Reference yield: 61.9%

5,6-diamino-3-methyl-1-phenyluracil (50786-93-1) + 3-acetyloxy-4-methylbenzoic acid (17477-46-2) → acetic acid 5-(6-amino-3-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylcarbamoyl)-2-methyl-phenyl ester (301206-04-2)

Guidance literature:

With triethylamine; Diphenylphosphinic chloride; In dichloromethane; at 0 ℃;

DOI:10.1016/S0968-0896(00)00126-7

upstream raw materials:

3-hydroxy-4-methylbenzoic acid

acetic anhydride

Downstream raw materials:

acetic acid 5-(6-amino-3-methyl-2,4-dioxo-1-phenyl-1,2,3,4-tetrahydro-pyrimidin-5-ylcarbamoyl)-2-methyl-phenyl ester

N-(4-chloro-phenyl)-3-hydroxy-4-methyl-benzamide

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