epocarbazolin A

Base Information

• Chemical Name: epocarbazolin A
• CAS No.: 146935-39-9
• Molecular Formula: C₂₂H₂₇NO₄
• Molecular Weight: 369.461
• Mol file: 146935-39-9.mol

Synonyms:9H-Carbazole-1,6-diol,4-(hydroxymethyl)-7-methyl-8-[3-methyl-3-(3-methylbutyl)oxiranyl]- (9CI);Epocarbazolin A

Chemical Property of epocarbazolin A

Chemical Property:

• Vapor Pressure: 4.52E-17mmHg at 25°C
• Boiling Point: 636.4°Cat760mmHg
• Flash Point: 338.7°C
• PSA: 89.01000
• Density: 1.283g/cm³
• LogP: 4.79920

Purity/Quality:

EPOCARBAZOLIN A 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of epocarbazolin A

There total 6 articles about epocarbazolin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

3,8-bis-(tert-butyl-diphenyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2-methyl-1-[3-methyl-3-(3-methyl-butyl)-oxiranyl]-9H-carbazole → (+/-)-epocarbazolin A (146935-39-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2006.06.095

Reference yield: 13.0%

3,8-bis-(tert-butyl-diphenyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxymethyl)-1-(2,5-dimethyl-hex-1-enyl)-2-methyl-9H-carbazole (909708-77-6) → (+/-)-epocarbazolin A (146935-39-9)

Guidance literature:

With tetrabutyl ammonium fluoride; 3,3-dimethyldioxirane;

DOI:10.1007/s00044-007-9073-0

Reference yield:

(-)-tri-O-(tert-butyldiphenylsilyl)epocarbazolin A → (-)-epocarbazolin A (146935-39-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2006.06.095

upstream raw materials:

3,8-bis-(tert-butyl-diphenyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxymethyl)-1-(2,5-dimethyl-hex-1-enyl)-2-methyl-9H-carbazole

[1,6-bis-(tert-butyl-diphenyl-silanyloxy)-8-(2,5-dimethyl-hex-1-enyl)-7-methyl-9H-carbazol-4-yl]-methanol

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