4-Decynal

Base Information

• Chemical Name: 4-Decynal
• CAS No.: 17522-26-8
• Molecular Formula: C10H16O
• Molecular Weight: 152.236
• Mol file: 17522-26-8.mol

Synonyms:

Chemical Property of 4-Decynal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Decynal

There total 1 articles about 4-Decynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

1-Heptyne (628-71-7) + acrolein (107-02-8,25068-14-8) → 2-pentyl-2-cyclopenten-1-one (25564-22-1) + 4-decyn-1-al (17522-26-8)

Guidance literature:

Co₂Rh₂ nanoparticles immobilized on charcoal; In tetrahydrofuran; at 130 ℃; for 18h;

DOI:10.1021/ol049765s

Reference yield: 67.0%

4-decyn-1-al (17522-26-8) + Cyclohexylmethyl bromide (2550-36-9) → 1-cyclohexyl-5-undecyn-2-ol

Guidance literature:

Cyclohexylmethyl bromide; With magnesium; In diethyl ether; for 0.5h; Reflux;

4-decyn-1-al; In diethyl ether; at -78 ℃; for 1h;

DOI:10.1021/acs.orglett.6b01392

Reference yield:

4-decyn-1-al (17522-26-8) → C17H31NO3S

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether / 0.5 h / Reflux

1.2: 1 h / -78 °C

2.1: formic acid; isocyanate de chlorosulfonyle / acetonitrile; N,N-dimethyl acetamide / 1 h / 20 °C

With formic acid; isocyanate de chlorosulfonyle; magnesium; In diethyl ether; N,N-dimethyl acetamide; acetonitrile;

DOI:10.1021/acs.orglett.6b01392

upstream raw materials:

1-Heptyne

acrolein

Downstream raw materials:

(Z)-undec-5-en-2-one