2-(2-Iodoanilino)-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-(2-Iodoanilino)-3,1-benzoxazin-4-one
CAS No.:178468-14-9
Molecular Formula:C14H9IN2O2
Molecular Weight:364.142
Hs Code.:
DSSTox Substance ID:DTXSID10439807
Nikkaji Number:J944.569B
Wikidata:Q82255889
ChEMBL ID:CHEMBL276438

Synonyms:CHEMBL276438;2-(2-iodoanilino)-3,1-benzoxazin-4-one;178468-14-9;SCHEMBL7339597;DTXSID10439807;BDBM50063715;2-[(2-Iodophenyl)amino]-4H-3,1-benzoxazin-4-one;2-(2-Iodo-phenylamino)-benzo[d][1,3]oxazin-4-one

Suppliers and Price of 2-(2-Iodoanilino)-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(2-Iodoanilino)-3,1-benzoxazin-4-one

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:363.97088
Heavy Atom Count:19
Complexity:386

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)OC(=N2)NC3=CC=CC=C3I

Technology Process of 2-(2-Iodoanilino)-3,1-benzoxazin-4-one

There total 4 articles about 2-(2-Iodoanilino)-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 194155-26-5
2-[3-(2-Iodo-phenyl)-ureido]-benzoic acid ethyl ester

: 178468-14-9
2-(2-Iodo-phenylamino)-benzo[d][1,3]oxazin-4-one

Guidance literature:: With sulfuric acid; at 50 ℃; for 1h;
DOI:10.1021/jm970394d

Reference yield:

: 128255-31-2
2-iodophenyl isocyanate

: 178468-14-9
2-(2-Iodo-phenylamino)-benzo[d][1,3]oxazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / tetrahydrofuran / 24 h / Ambient temperature

2: 86 percent / conc. sulfuric acid / 1 h / 50 °C

With sulfuric acid; In tetrahydrofuran;
DOI:10.1021/jm970394d

Reference yield:

: 128414-04-0,131152-15-3
2-iodoaniline hydrochloride

: 178468-14-9
2-(2-Iodo-phenylamino)-benzo[d][1,3]oxazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / toluene / 13 h / Heating

2: 78 percent / tetrahydrofuran / 24 h / Ambient temperature

3: 86 percent / conc. sulfuric acid / 1 h / 50 °C

With sulfuric acid; In tetrahydrofuran; toluene;
DOI:10.1021/jm970394d