4β-(1,5-Dimethyl-3-oxohexyl)cyclohexane-1β-carboxylic acid methyl ester

Base Information

• Chemical Name: 4β-(1,5-Dimethyl-3-oxohexyl)cyclohexane-1β-carboxylic acid methyl ester
• CAS No.: 17904-29-9
• Molecular Formula: C₁₆H₂₈O₃
• Molecular Weight: 268.397
• Mol file: 17904-29-9.mol

Synonyms:

Chemical Property of 4β-(1,5-Dimethyl-3-oxohexyl)cyclohexane-1β-carboxylic acid methyl ester

Chemical Property:

• PSA: 43.37000
• LogP: 3.60720

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4β-(1,5-Dimethyl-3-oxohexyl)cyclohexane-1β-carboxylic acid methyl ester

There total 5 articles about 4β-(1,5-Dimethyl-3-oxohexyl)cyclohexane-1β-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-Δ10-dehydroepijuvabione (65621-12-7) → 4-(1,5-Dimethyl-3-oxo-hexyl)-cyclohexanecarboxylic acid methyl ester (17904-29-9,17909-96-5,38963-60-9,57495-79-1,59202-69-6,59202-70-9,84680-64-8,125072-74-4,125072-76-6)

Guidance literature:

With hydrogen; acetic acid; Rh on carbon; In ethyl acetate; for 4h; under 715 Torr; Ambient temperature;

DOI:10.1016/S0040-4020(01)91308-0

Reference yield:

(+)-Δ7-dehydrojuvabione (64314-13-2) → 4-(1,5-Dimethyl-3-oxo-hexyl)-cyclohexanecarboxylic acid methyl ester (17904-29-9,17909-96-5,38963-60-9,57495-79-1,59202-69-6,59202-70-9,84680-64-8,125072-74-4,125072-76-6)

Guidance literature:

With hydrogen; acetic acid; Rh on carbon; In ethyl acetate; for 4h; under 715 Torr; Ambient temperature;

DOI:10.1016/S0040-4020(01)91308-0

Reference yield:

(+)-Δ10-dehydroepitodomatuic acid (93888-57-4) → 4-(1,5-Dimethyl-3-oxo-hexyl)-cyclohexanecarboxylic acid methyl ester (17904-29-9,17909-96-5,38963-60-9,57495-79-1,59202-69-6,59202-70-9,84680-64-8,125072-74-4,125072-76-6)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂, AcOH / Rh-C / ethyl acetate / 4 h / 715 Torr / Ambient temperature

With hydrogen; acetic acid; Rh on carbon; In ethyl acetate;

DOI:10.1016/S0040-4020(01)91308-0

upstream raw materials:

(+)-Δ¹⁰-dehydroepijuvabione

(+)-Δ⁷-dehydrojuvabione

(+)-Δ¹⁰-dehydroepitodomatuic acid

7-hydroxyjuvabione