Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)-

Base Information

Chemical Name:Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)-
CAS No.:17938-30-6
Molecular Formula:C15H20N2Si
Molecular Weight:256.423
Hs Code.:
Mol file:17938-30-6.mol

Synonyms:N',N'-diphenyl-N-trimethylsilylhydrazine;N.N-Diphenyl-N'-trimethylsilyl-hydrazin;

Suppliers and Price of Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)-

Chemical Property:

PSA：15.27000
LogP:4.55510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)-

There total 1 articles about Hydrazine, 1,1-diphenyl-2-(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17938-30-6
N,N-diphenyl-N'-(trimethylsilyl)hydrazine

Guidance literature:: N,N-Diphenyl-hydrazin, Li, Brombenzol, Trimethylchlorsilan;
DOI:10.1002/zaac.19613100105

Reference yield: 85.9%

: 17938-30-6
N,N-diphenyl-N'-(trimethylsilyl)hydrazine

: trimeric N-lithio-N',N'-diphenyl-N-(trimethylsilyl)hydrazine

Guidance literature:: With n-butyllithium; In hexane; for 14h;
DOI:10.1002/cber.19961291105

Reference yield: 56.0%

: 60-29-7,927820-24-4
diethyl ether

: 1184-58-3
dimethylaluminum chloride

: 17938-30-6
N,N-diphenyl-N'-(trimethylsilyl)hydrazine

: 219923-19-0
dimethylaluminium N',N'-diphenyl-N-trimethylsilylhydrazide-diethyl ether

Guidance literature:: With nBuLi; In diethyl ether; hexane; n-heptane; byproducts: butane, LiCl; Ar atmosphere, addn. of hexane soln. of nBuLi to Et2O soln. of hydrazinewith stirring, reflux (1 h), addn. of heptane soln. of AlMe2Cl at -69.d egree.C, warming to room temp., stirring (12 h); removement of solvent (vacuum), dissolution (hexane), filtration, crystn. (-20°C, 4 weeks); elem. anal.;