2-(2-Aminoethoxy)-1,3-dichlorobenzene

Base Information

Chemical Name:2-(2-Aminoethoxy)-1,3-dichlorobenzene
CAS No.:17944-28-4
Molecular Formula:C8H9Cl2NO
Molecular Weight:206.072
Hs Code.:
DSSTox Substance ID:DTXSID10582100
Wikidata:Q82473421
Mol file:17944-28-4.mol

Synonyms:17944-28-4;2-(2-Aminoethoxy)-1,3-dichlorobenzene;2-(2,6-dichlorophenoxy)ethanamine;2-(2,6-Dichlorophenoxy)ethan-1-amine;Ethanamine, 2-(2,6-dichlorophenoxy)-;SCHEMBL10927084;DTXSID10582100;AKOS008953647;SB78019;CS-0299753;EN300-1966547

Suppliers and Price of 2-(2-Aminoethoxy)-1,3-dichlorobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(2-Aminoethoxy)-1,3-dichlorobenzene

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:205.0061193
Heavy Atom Count:12
Complexity:124

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)OCCN)Cl

Technology Process of 2-(2-Aminoethoxy)-1,3-dichlorobenzene

There total 4 articles about 2-(2-Aminoethoxy)-1,3-dichlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 26646-21-9
N-[2-(2,6-dichlorophenoxy)ethyl]phthalimide

: 17944-28-4
2-(2,6-dichlorophenoxy)ethanamine

Guidance literature:: With hydrazine hydrate; In 2-methoxy-ethanol; for 2h; Heating;
DOI:10.1016/j.ejmech.2006.04.004

Reference yield:

: 914454-61-8
1-mesyloxy-2-(2,6-dichlorophenoxy)ethane

: 17944-28-4
2-(2,6-dichlorophenoxy)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / dimethylformamide / 1.5 h / 100 °C

2: 89 percent / hydrazine hydrate / 2-methoxy-ethanol / 2 h / Heating

With hydrazine hydrate; In 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.04.004

Reference yield:

: 42001-44-5
2-(2,6-dichlorophenoxy)ethanol

: 17944-28-4
2-(2,6-dichlorophenoxy)ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 87.8 percent / triethylamine / CH₂Cl₂ / 1 h / 20 °C

2: 39 percent / dimethylformamide / 1.5 h / 100 °C

3: 89 percent / hydrazine hydrate / 2-methoxy-ethanol / 2 h / Heating

With hydrazine hydrate; triethylamine; In dichloromethane; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.04.004