Carbamic acid, [(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]- 2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]- 2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester
CAS No.:179747-00-3
Molecular Formula:C24H32N4O6S
Molecular Weight:504.607
Hs Code.:

Carbamic acid,
[(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]-
2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]- 2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]- 2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester

There total 4 articles about Carbamic acid, [(1S)-1-[[4-[imino[[(4-methylphenyl)sulfonyl]amino]methyl]phenyl]methyl]- 2-(methoxymethylamino)-2-oxoethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2-(4-carbamimidoyl-phenyl)-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester; hydriodide

: 98-59-9
p-toluenesulfonyl chloride

: 179747-00-3
[2-{4-[imino-(toluene-4-sulfonylamino)-methyl]-phenyl}-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetone; at -15 - 20 ℃; for 3h;
DOI:10.1021/jm0303857

Reference yield:

: 179746-96-4
[2-(4-cyano-phenyl)-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester

: 179747-00-3
[2-{4-[imino-(toluene-4-sulfonylamino)-methyl]-phenyl}-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / H₂S(gas); Et₃H; pyridine / 72 h

2: acetone / 1 h / Heating

3: ammonium acetate / methanol / 3.5 h / Heating

4: 14.4 g / DBU / acetone / 3 h / -15 - 20 °C

With pyridine; ammonium acetate; hydrogen sulfide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; acetone;
DOI:10.1021/jm0303857

Reference yield:

: 179746-97-5
[1-(methoxy-methyl-carbamoyl)-2-(4-thiocarbamoyl-phenyl)-ethyl]-carbamic acid tert-butyl ester

: 179747-00-3
[2-{4-[imino-(toluene-4-sulfonylamino)-methyl]-phenyl}-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 1 h / Heating

2: ammonium acetate / methanol / 3.5 h / Heating

3: 14.4 g / DBU / acetone / 3 h / -15 - 20 °C

With ammonium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; acetone;
DOI:10.1021/jm0303857