4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester
CAS No.:182576-32-5
Molecular Formula:C29H34N6O11S2
Molecular Weight:706.755
Hs Code.:
Mol file:182576-32-5.mol

4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-
8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl
ester

Synonyms:

Suppliers and Price of 4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester

There total 3 articles about 4-Oxa-3,8,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene- 8-carboxylic acid, 3,11-bis[(2-nitrophenyl)sulfonyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 7703-74-4
2,6-bis-(bromomethyl)pyridine

: 182576-30-3
[2-(2-Nitro-benzenesulfonylamino)-ethyl]-[3-(2-nitro-benzenesulfonylaminooxy)-propyl]-carbamic acid tert-butyl ester

: 182576-32-5
3,11-Bis-(2-nitro-benzenesulfonyl)-4-oxa-3,8,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-triene-8-carboxylic acid tert-butyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1016/0040-4039(96)01627-9 DOI:10.1021/ja964153r

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 182576-32-5
3,11-Bis-(2-nitro-benzenesulfonyl)-4-oxa-3,8,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-triene-8-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 50 percent / Cs₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja964153r

Reference yield:

: 182576-29-0
(2-aminoethyl)(3-aminooxypropyl)carbamic acid tert-butyl ester

: 182576-32-5
3,11-Bis-(2-nitro-benzenesulfonyl)-4-oxa-3,8,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-triene-8-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 50 percent / Cs₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja964153r