2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-

Base Information

Chemical Name:2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-
CAS No.:183023-15-6
Molecular Formula:C10H9NO2
Molecular Weight:175.187
Hs Code.:
DSSTox Substance ID:DTXSID20449174
Nikkaji Number:J767.518F
Wikidata:Q82268556
Mol file:183023-15-6.mol

Synonyms:2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-;183023-15-6;DTXSID20449174;5beta-Phenyl-5,6-dihydro-2H-1,4-oxazine-2-one;(5s)-5-phenyl-5,6-dihydro-2h-1,4-oxazin-2-one

Suppliers and Price of 2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:175.063328530
Heavy Atom Count:13
Complexity:219

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(N=CC(=O)O1)C2=CC=CC=C2
Isomeric SMILES:C1[C@@H](N=CC(=O)O1)C2=CC=CC=C2

Technology Process of 2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)-

There total 3 articles about 2H-1,4-Oxazin-2-one, 5,6-dihydro-5-phenyl-, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 222622-39-1
(4S)-4,5-dihydro-2-methyl-4-phenyl-1,3-oxazole

: 183023-15-6
(S)-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; at 110 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ol1001126

Reference yield: 55.0%

: 144896-92-4,134872-85-8
(5S)-5-phenylmorpholin-2-one

: 183023-15-6
(S)-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: With N-Bromosuccinimide; methyloxirane; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/0957-4166(96)00329-1

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 183023-15-6
(S)-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 16 h / 0 - 40 °C

2: selenium(IV) oxide / tetrahydrofuran / 2 h / 85 °C / Inert atmosphere

With selenium(IV) oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol502045u