ilexsaponin B1

Base Information

• Chemical Name: ilexsaponin B1
• CAS No.: 109008-27-7
• Molecular Formula: C₄₁H₆₆O₁₃
• Molecular Weight: 766.967
• Mol file: 109008-27-7.mol

Synonyms:Ilexoside D;ilexsaponin B1;

Chemical Property of ilexsaponin B1

Chemical Property:

• PSA: 215.83000
• LogP: 2.49190

Purity/Quality:

98% ^*data from raw suppliers

Ilexoside D ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ilexsaponin B1

There total 2 articles about ilexsaponin B1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ilexsaponin B2 (108906-69-0) → ilexsaponin B1 (83725-19-3,109008-27-7) + ilexgenin B (13849-91-7,19870-71-4,109008-39-1,119067-01-5) + prosapogenin (35286-59-0,108544-40-7,109008-40-4)

Guidance literature:

With hesperidinase; In toluene; at 37 ℃; for 48h; Product distribution;

DOI:10.1248/cpb.35.524

Reference yield:

ilexsaponin B3 (88255-95-2,109008-26-6) → methyl D-glucopyranoside (97-30-3,617-04-9,709-50-2,1824-94-8,2152-78-5,3396-99-4,6819-48-3,18469-06-2,20550-04-3,22277-65-2,29411-57-2,35437-40-2,35437-43-5,36191-11-4,36191-12-5,39598-79-3,39598-80-6,39598-89-5,51023-63-3,51223-62-2,51224-38-5,51224-39-6,51224-40-9,51224-41-0,51819-81-9,51819-82-0,51819-83-1,56688-81-4,62279-53-2,64281-79-4,64281-80-7,64912-19-2,66101-73-3,78184-90-4,84368-39-8,84368-40-1,84368-41-2,92142-37-5,93302-26-2,103421-28-9,115794-08-6,3149-68-6) + ilexsaponin B1 (83725-19-3,109008-27-7)

Guidance literature:

With lithium iodide; In methanol; for 13h; Product distribution; Heating;

DOI:10.1248/cpb.35.524

Reference yield:

ilexsaponin B1 (83725-19-3,109008-27-7) → ilexgenin B (13849-91-7,19870-71-4,109008-39-1,119067-01-5) + prosapogenin (35286-59-0,108544-40-7,109008-40-4)

Guidance literature:

With hesperidinase; In various solvent(s); at 38 ℃; for 90h; Yield given. Yields of byproduct given;

DOI:10.1248/cpb.35.524

upstream raw materials:

ilexsaponin B₂

ilexsaponin B₃

Downstream raw materials:

ilexgenin B

prosapogenin

(1R,2S,4aS,6aS,6bR,10S,12aR,14bS)-1,10-Dihydroxy-1,2,6a,6b,9,9,12a-heptamethyl-1,3,4,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-octadecahydro-2H-picene-4a-carboxylic acid methyl ester

Refernces