beta-Chloro-p-methylcinnamaldehyde

Base Information

Chemical Name:beta-Chloro-p-methylcinnamaldehyde
CAS No.:40808-08-0
Molecular Formula:C10H9ClO
Molecular Weight:180.634
Hs Code.:
Nikkaji Number:J2.094.721G
Wikidata:Q76325920
Mol file:40808-08-0.mol

Synonyms:beta-Chloro-p-methylcinnamaldehyde;BRN 2638109;CINNAMALDEHYDE, beta-CHLORO-p-METHYL-;40808-08-0;SCHEMBL6708832;SCHEMBL17268780;AKOS017514967;(Z)-beta-Chloro-4-methylbenzenepropenal;LS-53827

Suppliers and Price of beta-Chloro-p-methylcinnamaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of beta-Chloro-p-methylcinnamaldehyde

Chemical Property:

Vapor Pressure:0.00258mmHg at 25°C
Boiling Point:286.8°Cat760mmHg
Flash Point:142.9°C
Density:1.137g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:180.0341926
Heavy Atom Count:12
Complexity:178

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=CC=O)Cl
Isomeric SMILES:CC1=CC=C(C=C1)/C(=C/C=O)/Cl

Technology Process of beta-Chloro-p-methylcinnamaldehyde

There total 5 articles about beta-Chloro-p-methylcinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18103-98-5
3-dimethylamino-1-(4-methyl-phenyl)-2-propen-1-one

: 40808-08-0
(Z)-3-chloro-3-(p-tolyl)acrylaldehyde

Guidance literature:: 3-dimethylamino-1-(4-methyl-phenyl)-2-propen-1-one; With trichlorophosphate; In dichloromethane; for 2h; Reflux;

With water; In tetrahydrofuran; at 20 ℃; for 24h; diastereoselective reaction;
DOI:10.1016/j.tet.2010.09.080

Reference yield: 80.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 122-00-9
para-methylacetophenone

: 40808-08-0
(Z)-3-chloro-3-(p-tolyl)acrylaldehyde

Guidance literature:: N,N-dimethyl-formamide; With bis(trichloromethyl) carbonate; In chloroform; at 20 ℃; Cooling with ice;

para-methylacetophenone; In chloroform; at 20 - 60 ℃;
DOI:10.1080/00397910903262187

Reference yield: 72.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 122-00-9
para-methylacetophenone

: 40808-08-0
1-Chlor-1-p-tolyl-propen-3-al

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

para-methylacetophenone; at 0 - 65 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c1cc13908h