2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid

Base Information

Chemical Name:2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid
CAS No.:25556-24-5
Molecular Formula:C29H36 O9
Molecular Weight:528.5907
Hs Code.:
Mol file:25556-24-5.mol

Synonyms:b-Resorcylic acid,6-(2-oxoheptyl)-, ester with 4-hydroxy-6-(2-oxoheptyl)-o-anisic acid (8CI);Arthonia acid; Arthoniaic acid

Suppliers and Price of 2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid

Chemical Property:

Vapor Pressure:7.85E-21mmHg at 25°C
Boiling Point:704.5°Cat760mmHg
Flash Point:226.3°C
PSA：147.43000
Density:1.225g/cm³
LogP:5.40760

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid

There total 15 articles about 2-Methoxy-4-[2-(2-oxoheptyl)-4,6-dihydroxybenzoyloxy]-6-(2-oxoheptyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 193617-69-5
benzyl arthoniaiate

: 25556-24-5
Arthoniasaeure

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h;
DOI:10.1071/C96173

Reference yield:

: 646-14-0
1-nitrohexane

: 25556-24-5
Arthoniasaeure

Guidance literature:: Multi-step reaction with 11 steps

1: 63.5 percent / butylamine / toluene / 27 h / Heating

2: 1.) hydrogen; 2.) sodium metabisulfite / 1.) 10percent palladium on carbon / 1.) glacial AcOH, EtOAc, 63 h; 2.) aq. EtOH, 3 h, reflux

3: 22 percent / titanium(IV) chloride / CH₂Cl₂ / 0.12 h / Ambient temperature

4: 25 g / sodium hydrogen carbonate / dimethylformamide / 24 h

5: 61 percent / sodium hydrogen carbonate / dimethylformamide / 23 h / Ambient temperature

6: sulfamic acid, aq. sodium chlorite / dioxane / 1.2 h / Ambient temperature

7: hydrogen / 10percent palladium on carbon / ethyl acetate / 18 h

8: sodium hydrogen carbonate / dimethylformamide / 23.5 h / Ambient temperature

9: 61 percent / dicyclohexylcarbodiimide / toluene / 1 h / Ambient temperature

10: 31 percent / 5 M HCl / methanol / Ambient temperature

11: 88 percent / hydrogen / 10percent palladium on carbon / ethyl acetate / 16 h

With hydrogenchloride; sodium chlorite; sodium disulfite; aminosulfonic acid; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; N-butylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C96173

Reference yield:

: 15601-09-9
1-(3',5'-dihydroxyphenyl)heptan-2-one

: 25556-24-5
Arthoniasaeure

Guidance literature:: Multi-step reaction with 9 steps

1: 22 percent / titanium(IV) chloride / CH₂Cl₂ / 0.12 h / Ambient temperature

2: 25 g / sodium hydrogen carbonate / dimethylformamide / 24 h

3: 61 percent / sodium hydrogen carbonate / dimethylformamide / 23 h / Ambient temperature

4: sulfamic acid, aq. sodium chlorite / dioxane / 1.2 h / Ambient temperature

5: hydrogen / 10percent palladium on carbon / ethyl acetate / 18 h

6: sodium hydrogen carbonate / dimethylformamide / 23.5 h / Ambient temperature

7: 61 percent / dicyclohexylcarbodiimide / toluene / 1 h / Ambient temperature

8: 31 percent / 5 M HCl / methanol / Ambient temperature

9: 88 percent / hydrogen / 10percent palladium on carbon / ethyl acetate / 16 h

With hydrogenchloride; sodium chlorite; aminosulfonic acid; hydrogen; titanium tetrachloride; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1071/C96173